Preparation and evaluation of a novel chiral stationary phase based on covalently bonded chitosan for ligand-exchange chromatography
文献类型：期刊论文
| 作者 | Liu, Yueqi; Zou, Hanfa; Haginaka, Jun |
| 刊名 | journal of separation science
 |
| 出版日期 | 2006-07-01 |
| 卷号 | 29期号:10页码:1440-1446 |
| 关键词 | alpha-amino acids alpha-hydroxycarboxylic acids chiral stationary phase chitosan ligand-exchange liquid chromatography |
| ISSN号 | 1615-9306 |
| 产权排序 | 2;1 |
| 通讯作者 | 邹汉法 ; jun haginaka |
| 英文摘要 | a novel chiral stationary phase based on chitosan covalently bonded onto silica gels has been prepared and used for the separation of various alpha-amino acid enantiomers as well as alpha-hydroxycarboxylic acid enantiomers by chiral ligand-exchange chromatography with copper(ii) as a complexing ion. the methanol content and copper(ii) ion concentration in the eluent affected retentivity and enantioselectivity. furthermore, a plausible chiral recognition mechanism for resolution of alpha-amino acids was proposed. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | performance liquid-chromatography ; amino-acids ; alpha-amino ; carbamate derivatives ; optical isomers ; separation ; chitin ; resolution ; selectors ; silica |
| 收录类别 | SCI |
| 原文出处 | true |
| 语种 | 英语 |
| WOS记录号 | WOS:000239291200016 |
| 公开日期 | 2010-11-30 |
| 源URL | [http://159.226.238.44/handle/321008/93859]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Mukogawa Womens Univ, Fac Pharmaceut Sci, Nishinomiya, Hyogo 6638179, Japan 2.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian, Peoples R China |
| 推荐引用方式 GB/T 7714 | Liu, Yueqi,Zou, Hanfa,Haginaka, Jun. Preparation and evaluation of a novel chiral stationary phase based on covalently bonded chitosan for ligand-exchange chromatography[J]. journal of separation science,2006,29(10):1440-1446. |
| APA | Liu, Yueqi,Zou, Hanfa,&Haginaka, Jun.(2006).Preparation and evaluation of a novel chiral stationary phase based on covalently bonded chitosan for ligand-exchange chromatography.journal of separation science,29(10),1440-1446. |
| MLA | Liu, Yueqi,et al."Preparation and evaluation of a novel chiral stationary phase based on covalently bonded chitosan for ligand-exchange chromatography".journal of separation science 29.10(2006):1440-1446. |
入库方式： OAI收割
来源：大连化学物理研究所
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