On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum
文献类型：期刊论文
| 作者 | Zhang, Jie; Zhang, Lihua; Duan, Jicheng; Liang, Zhen; Zhang, Weibing; Hu, Yushu; Zhang, Yukui |
| 刊名 | journal of separation science
 |
| 出版日期 | 2006-11-01 |
| 卷号 | 29期号:16页码:2514-2522 |
| 关键词 | Ganoderma lucidum mass spectrometry natural products supercritical fluid extraction |
| 产权排序 | 1;1 |
| 通讯作者 | 张丽华 |
| 英文摘要 | a novel on-line system combining supercritical fluid extraction (sfe) and two-dimensional high performance liquid chromatography (2d-hplc) was developed. a trap column and two three-port valves were employed to couple sfe and 2d-hplc system, which was composed of a cn column and a monolithic silica column, connected by a 10-port dual-position valve. the analytes extracted by supercritical co2 were completely transferred to the 2d-hplc system. after separation in two orthogonal modes, the eluents were delivered to apci-tandem-ms for identification of the samples. in this way, sample preparation, separation, detection, and identification were integrated into an on-line system permitting analysis of the fruiting bodies of ganoderma lucidum, and at least 73 components in the extract were resolved with calculated peak capacity of up to 1643. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | aromatic-hydrocarbons ; quantitative-analysis ; hplc system ; separation ; matrices ; triacylglycerols ; products ; column |
| 收录类别 | SCI |
| 原文出处 | true |
| 语种 | 英语 |
| WOS记录号 | WOS:000242242300013 |
| 公开日期 | 2010-11-30 |
| 源URL | [http://159.226.238.44/handle/321008/97575]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian, Peoples R China 2.Univ Texas, Hlth Sci Ctr, San Antonio, TX 78285 USA |
| 推荐引用方式 GB/T 7714 | Zhang, Jie,Zhang, Lihua,Duan, Jicheng,et al. On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum[J]. journal of separation science,2006,29(16):2514-2522. |
| APA | Zhang, Jie.,Zhang, Lihua.,Duan, Jicheng.,Liang, Zhen.,Zhang, Weibing.,...&Zhang, Yukui.(2006).On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum.journal of separation science,29(16),2514-2522. |
| MLA | Zhang, Jie,et al."On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum".journal of separation science 29.16(2006):2514-2522. |
入库方式： OAI收割
来源：大连化学物理研究所
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