High pressure single-crystal synchrotron x-ray diffraction technique
文献类型：期刊论文
| 作者 | Li Xiao-Dong1; Li Hui2; Li Peng-Shan1 |
| 刊名 | Acta physica sinica
 |
| 出版日期 | 2017-02-01 |
| 卷号 | 66期号:3页码:13 |
| 关键词 | High pressure Single-crystal Synchrotron radiation X-ray diffraction |
| ISSN号 | 1000-3290 |
| DOI | 10.7498/aps.66.036203 |
| 通讯作者 | Li xiao-dong(lixd@ihep.ac.cn) |
| 英文摘要 | A lot of great work has been done since the high pressure research carried out on synchrotron radiation facility almost 40 years ago. the history of high pressure single-crystal diffraction research on synchrotron radiation facility has also been more than 20 years. recently, with the development of synchrotron x-ray optical techniques and high pressure technology, especially the invention and improvement of large opening diamond anvil cell (dac), high pressure single-crystal x-ray diffraction (hpsxrd) method has become more and more popular in high pressure studies. the hpsxrd can be used to perform structure determination and refinement to obtain the information about lattice parameter, space group, atomic coordinate and site occupation. compared with powder x-ray diffraction, the hpsxrd can not only obtain the three-dimensional diffraction information of samples, but also have much better signal-to-noise ratio. furthermore, the hpsxrd data can be used to study the electron density distribution to obtain more information about chemical bonds and electron distribution. in this work, we introduce the hpsxrd method in synchrotron radiation facilities, including the knowledge of single-crystal x-ray diffraction experimental system, dac for hpsxrd, sample loading, and hpsxrd data processing. |
| WOS关键词 | DIAMOND-ANVIL CELL ; GAS-LOADING SYSTEM ; EXTREME CONDITIONS ; HYDROSTATIC LIMITS ; SILICONE FLUID ; 10 GPA ; SUPERCONDUCTIVITY ; STATE ; CRYSTALLOGRAPHY ; GIGAPASCALS |
| WOS研究方向 | Physics |
| WOS类目 | Physics, Multidisciplinary |
| 语种 | 英语 |
| WOS记录号 | WOS:000397300600018 |
| 出版者 | CHINESE PHYSICAL SOC |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2176705 |
| 专题 | 高能物理研究所 |
| 通讯作者 | Li Xiao-Dong |
| 作者单位 | 1.Chinese Acad Sci, Inst High Energy Phys, Ctr Multidisciplinary Res, Beijing 100049, Peoples R China 2.Beijing Univ Technol, Inst Microstruct & Properties Adv Mat, Beijing 100124, Peoples R China |
| 推荐引用方式 GB/T 7714 | Li Xiao-Dong,Li Hui,Li Peng-Shan. High pressure single-crystal synchrotron x-ray diffraction technique[J]. Acta physica sinica,2017,66(3):13. |
| APA | Li Xiao-Dong,Li Hui,&Li Peng-Shan.(2017).High pressure single-crystal synchrotron x-ray diffraction technique.Acta physica sinica,66(3),13. |
| MLA | Li Xiao-Dong,et al."High pressure single-crystal synchrotron x-ray diffraction technique".Acta physica sinica 66.3(2017):13. |
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来源：高能物理研究所
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