Characterization of caffeoylquinic acids from Hedyotis diffusa by liquid chromatography/ tandem mass spectrometry
文献类型:会议论文
作者 | Li CM(李存满) ; Xue XY(薛兴亚) ; Zhang FF(章飞芳) ; Xu Q(徐青) ; Liang XM(梁鑫淼) |
出版日期 | 2007-06-04 |
会议名称 | dalian international symposia and exhibition on chromatography |
会议日期 | 2007-6-4 |
会议地点 | 中国 |
页码 | 10/1 |
通讯作者 | 梁鑫淼 |
中文摘要 | a high-performance liquid chromatography-uv/dad combined with electrospray ionization tandem mass spectrometry method (hplc-uv/dad-esi-ms/ms) was described for the characterization of caffeoylquinic acids from hedyotis diffusa. the optimized separation and ionization efficiency for the compounds studied was obtained when using ch3oh/h2o eluent system with 0.1% formic acid as the additive. in this work, three isomers of caffeoylquinic acids, to our knowledge, were observed from hedyotis diffusa for the first time. based on the uv spectra and fragmentation of the three isomers in positive and negative ion modes and compared with literatures, they were tentatively identified as 3-o-caffeoylquinic acid, 5-o-caffeoylquinic acid and 4-o-caffeoylquinic acid, respectively. |
会议主办者 | 中国科学院大连化学物理研究所 |
学科主题 | 物理化学 |
语种 | 中文 |
源URL | [http://159.226.238.44/handle/321008/112474] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
推荐引用方式 GB/T 7714 | Li CM,Xue XY,Zhang FF,et al. Characterization of caffeoylquinic acids from Hedyotis diffusa by liquid chromatography/ tandem mass spectrometry[C]. 见:dalian international symposia and exhibition on chromatography. 中国. 2007-6-4. |
入库方式: OAI收割
来源:大连化学物理研究所
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