Synthesis of polycrystalline CoFe2O4 and NiFe2O4 powders by auto-combustion method using a novel amino-based gel
文献类型:期刊论文
作者 | Jiang, Linwen1; Yang, Shanshan; Zheng, Mengyao; Wu, Anhua2; Chen, Hongbing1 |
刊名 | MATERIALS RESEARCH EXPRESS
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出版日期 | 2017 |
卷号 | 4期号:12 |
ISSN号 | 2053-1591 |
DOI | 10.1088/2053-1591/aa9b10 |
英文摘要 | Polycrystalline CoFe2O4/NiFe2O4 powders were prepared by auto-combustion method using a novel amino-based gel. The thermal evolution of gel precursors, as well as the microstructure, morphology and magnetic properties of as-synthesized powders were studied in detail. Energy dispersive x-ray spectroscopy indicated that the ratios of Ni:Fe was close to the theoretical value (Ni:Fe = 1: 2), suggesting high purity of synthesized NiFe2O4 powders. The saturated magnetization (M-s) and residual magnetization (Mr) of CoFe2O4 were highly dependent upon the annealed temperatures. The Ms increased from 77.5 to 84.7 emu g(-1), and Mr increased from 37.7 emu g(-1) to 42.5 emu g(-1) by annealing from room temperature to 600 degrees C. The Ms of NiFe2O4 was 38.7 emu g(-1), much lower than that of CoFe2O4. The experimental results indicated that this auto-combustion method using amino-based gel was a suitable method for synthesizing high-quality CoFe2O4/NiFe2O4 powders. |
WOS记录号 | WOS:000417565800002 |
源URL | [http://ir.sic.ac.cn/handle/331005/26624] ![]() |
专题 | 中国科学院上海硅酸盐研究所 |
作者单位 | 1.Ningbo Univ, State Key Base Funct Mat & Preparat Sci, Ningbo 315211, Zhejiang, Peoples R China 2.Ningbo Univ, Key Lab Photoelect Detect Mat & Devices Zhejiang P, Ningbo 315211, Zhejiang, Peoples R China 3.Chinese Acad Sci, Shanghai Inst Ceram, Shanghai 201800, Peoples R China |
推荐引用方式 GB/T 7714 | Jiang, Linwen,Yang, Shanshan,Zheng, Mengyao,et al. Synthesis of polycrystalline CoFe2O4 and NiFe2O4 powders by auto-combustion method using a novel amino-based gel[J]. MATERIALS RESEARCH EXPRESS,2017,4(12). |
APA | Jiang, Linwen,Yang, Shanshan,Zheng, Mengyao,Wu, Anhua,&Chen, Hongbing.(2017).Synthesis of polycrystalline CoFe2O4 and NiFe2O4 powders by auto-combustion method using a novel amino-based gel.MATERIALS RESEARCH EXPRESS,4(12). |
MLA | Jiang, Linwen,et al."Synthesis of polycrystalline CoFe2O4 and NiFe2O4 powders by auto-combustion method using a novel amino-based gel".MATERIALS RESEARCH EXPRESS 4.12(2017). |
入库方式: OAI收割
来源:上海硅酸盐研究所
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