On-line immunoaffinity column-liquid chromatography-tandem mass spectrometry method for trace analysis of diuron in wastewater treatment plant effluent sample
文献类型：期刊论文
| 作者 | Zhang, Xiuli; Martens, Dieter; Kraemer, Petra M.; Kettrup, Antonius A.; Liang, Xinmiao |
| 刊名 | journal of chromatography a
 |
| 出版日期 | 2006-11-10 |
| 卷号 | 1133期号:1-2页码:112-118 |
| 关键词 | immunoaffinity column diuron on-line LC-MS-MS matrix effect wastewater |
| 产权排序 | 1;1 |
| 通讯作者 | 梁鑫淼 |
| 英文摘要 | an on-line immunoaffinity column with liquid chromatography/tandem mass spectrometry (iac-lc-ms/ms) method for the determination of diuron in water matrices was described. this method used a sol-gel immunoaffinity column (20 mm x 4 mm i.d.) for on-line sample cleanup and enrichment, a monolithic analytical column (100 mm x 4.6 mm i.d.) for separation, and a triple quadrupole mass spectrometer for quantitation. the major challenges for the on-line set-up were discussed. the optimized on-line protocol was emphasized by the fact that low limit of quantitation (loq) of 1.0 ng/l was achieved with only 2.5-ml sample. in addition, a satisfactory accuracy (similar to 90% of recovery) and precision (< 6% of relative standard deviation) at 50 ng/l concentration were also obtained. due to the ability of the sol-gel immunoaffinity column to eliminate matrix effect, the on-line iac-lc-ms/ms analysis method can reliably determine diuron in wastewater treatment plant effluent sample. (c) 2006 elsevier b.v. all rights reserved. |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 类目[WOS] | biochemical research methods ; chemistry, analytical |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | solid-phase extraction ; pesticide-residues ; transformation products ; emerging contaminants ; endocrine disruptors ; level determination ; gas-chromatography ; current issues ; surface-water ; s-triazines |
| 收录类别 | SCI |
| 原文出处 | true |
| 语种 | 英语 |
| WOS记录号 | WOS:000241772800014 |
| 公开日期 | 2010-11-30 |
| 源URL | [http://159.226.238.44/handle/321008/97791]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.LUFA Speyer, D-67346 Speyer, Germany 2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China 3.GSF, Inst Ecol Chem, Natl Res Ctr Environm & Hlth, D-85764 Neuherberg, Germany 4.Tech Univ Munich, Lehrstuhl Okol Chem & Umweltanalyt, D-85350 Freising Weihenstephan, Germany |
| 推荐引用方式 GB/T 7714 | Zhang, Xiuli,Martens, Dieter,Kraemer, Petra M.,et al. On-line immunoaffinity column-liquid chromatography-tandem mass spectrometry method for trace analysis of diuron in wastewater treatment plant effluent sample[J]. journal of chromatography a,2006,1133(1-2):112-118. |
| APA | Zhang, Xiuli,Martens, Dieter,Kraemer, Petra M.,Kettrup, Antonius A.,&Liang, Xinmiao.(2006).On-line immunoaffinity column-liquid chromatography-tandem mass spectrometry method for trace analysis of diuron in wastewater treatment plant effluent sample.journal of chromatography a,1133(1-2),112-118. |
| MLA | Zhang, Xiuli,et al."On-line immunoaffinity column-liquid chromatography-tandem mass spectrometry method for trace analysis of diuron in wastewater treatment plant effluent sample".journal of chromatography a 1133.1-2(2006):112-118. |
入库方式： OAI收割
来源：大连化学物理研究所
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