Synthesis and. crystal structure of N '-(4-fluorobenzylidene)-2-(1H-1,2,4-triazole-1-yl) acetohydrazide
文献类型：期刊论文
| 作者 | Li Wei-hua; Zhang Shu-fang; Hou Bao-rong; Yu Zhi-gang |
| 刊名 | CHEMICAL RESEARCH IN CHINESE UNIVERSITIES
 |
| 出版日期 | 2006-09-01 |
| 卷号 | 22期号:5页码:571-573 |
| 关键词 | Acetohydrazide 1h-1 Crystal Structure 2 Biological Activity 4-triazole |
| ISSN号 | 1005-9040 |
| 文献子类 | Article |
| 英文摘要 | N'-(4-fluorobenzylidene)-2-(1H-1 2,4-triazole-1-yl) acetohydrazide was synthesized by the reaction of 4-fluorobenzaldehyde with 2-(1H-1 2,4-triazole-1-yl) acetohydrazide. The structure was confirmed via elemental analysis, MS, H-1 NMR, IR, and X-ray diffraction. It crystallized in a monoclinic system with space group P2 (1) a = 0.4905 (1) nm, b = 0.8160 (2) nm, c = 1.4105 (3) nm, beta = 93.33 (3)degrees, Z = 2, V = 0.5636 (2) nm(3), D-c = 1.457 Mg/m(3), mu = 0.112 mm(-1), F(000) = 256, and final R-1 = 0.0685. Several intermolecular hydrogen-bond interactions existed in the crystal structure, facilitating the stabilization of the compound.; N'-(4-fluorobenzylidene)-2-(1H-1 2,4-triazole-1-yl) acetohydrazide was synthesized by the reaction of 4-fluorobenzaldehyde with 2-(1H-1 2,4-triazole-1-yl) acetohydrazide. The structure was confirmed via elemental analysis, MS, H-1 NMR, IR, and X-ray diffraction. It crystallized in a monoclinic system with space group P2 (1) a = 0.4905 (1) nm, b = 0.8160 (2) nm, c = 1.4105 (3) nm, beta = 93.33 (3)degrees, Z = 2, V = 0.5636 (2) nm(3), D-c = 1.457 Mg/m(3), mu = 0.112 mm(-1), F(000) = 256, and final R-1 = 0.0685. Several intermolecular hydrogen-bond interactions existed in the crystal structure, facilitating the stabilization of the compound. |
| 学科主题 | Chemistry, Multidisciplinary |
| 语种 | 英语 |
| WOS记录号 | WOS:000241048900007 |
| 公开日期 | 2010-12-24 |
| 源URL | [http://ir.qdio.ac.cn/handle/337002/5189]  |
| 专题 | 海洋研究所_海洋腐蚀与防护研究发展中心 |
| 作者单位 | 1.Ocean Univ China, Coll Chem & Chem Engn, Qingdao 266033, Peoples R China 2.Chinese Acad Sci, Inst Oceanol, Qingdao 266071, Peoples R China |
| 推荐引用方式 GB/T 7714 | Li Wei-hua,Zhang Shu-fang,Hou Bao-rong,et al. Synthesis and. crystal structure of N '-(4-fluorobenzylidene)-2-(1H-1,2,4-triazole-1-yl) acetohydrazide[J]. CHEMICAL RESEARCH IN CHINESE UNIVERSITIES,2006,22(5):571-573. |
| APA | Li Wei-hua,Zhang Shu-fang,Hou Bao-rong,&Yu Zhi-gang.(2006).Synthesis and. crystal structure of N '-(4-fluorobenzylidene)-2-(1H-1,2,4-triazole-1-yl) acetohydrazide.CHEMICAL RESEARCH IN CHINESE UNIVERSITIES,22(5),571-573. |
| MLA | Li Wei-hua,et al."Synthesis and. crystal structure of N '-(4-fluorobenzylidene)-2-(1H-1,2,4-triazole-1-yl) acetohydrazide".CHEMICAL RESEARCH IN CHINESE UNIVERSITIES 22.5(2006):571-573. |
入库方式： OAI收割
来源：海洋研究所
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