中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
From chain to layer structure: zn-ii coordination polymers derived from diphenic acid

文献类型:期刊论文

作者Wang, RH; Gong, YQ; Han, L; Yuan, DQ; Hong, MC
刊名Chinese journal of structural chemistry
出版日期2005
卷号24期号:9页码:1007-1016
关键词Diphenic acid Zinc Coordination polymers Crystal structure
ISSN号0254-5861
通讯作者Hong, mc()
英文摘要Three zn-ii coordination polymers, [zn(py)(h2o)(dpa)](n) 1, [zn-2(4,4'-bipy)(2)(dpa)(2)](n) 2 and [zn(bpe)(h2o)(2)(hdpa)(2)](n) 3 (py = pyridine, h(2)dpa = diphenic acid, 4,4'-bipy = 4,4'-bipyridine, bpe = 1,2-bis(4-pyridyl)ethane), were synthesized and characterized by x-ray single-crystal structure determination. 1 crystallizes in monoclinic, space group c2/c with a = 23.014(3), b = 8.7184(13), c = 18.091(3) angstrom, beta = 95.964(3)degrees, v = 3610.2(9) angstrom(3), z = 8, c19h15no5zn, m-r = 402.69, d-c = 1.482 g/cm(3), f(000) = 1648, mu(mok alpha) = 1.389 mm(-1), the final r = 0.0431 and wr = 0.1120 for 4239 observed reflections with 1 > 2 sigma(i). 2 crystallizes in orthorhombic, space group fddd with a = 23.1613(5), b = 24.0324(6), c = 29.4785(1) angstrom, v = 16408.4(5) angstrom(3), z = 32, c24h16n2o4zn, m-r = 461.76, d-c = 1.495 g/cm(3), f(000) = 7552, mu(mok alpha) = 1.232 mm(-1), the final r = 0.0542 and wr = 0.1724 for 3632 observed reflections with i > 2 sigma(i). 3 crystallizes in orthorhombic, space group c2/c with a = 19.142(4), b = 13.862(3), c = 15.625(3) angstrom, beta = 122.404(3)degrees, v 3500.3(11) a(3), z = 8, c20h17no5zn0.50, m-r = 384.03, d-c = 1.457 g/cm(3), f(000) = 1592, mu(mok alpha) 0.766 mm(-1), the final r = 0.0400 and wr = 0.1210 for 4024 observed reflections with i > 2 sigma(i).
WOS关键词CRYSTAL-STRUCTURE ; HELICAL CHAINS ; LIGANDS ; COMPLEXES ; FRAMEWORK ; COVALENT
WOS研究方向Chemistry ; Crystallography
WOS类目Chemistry, Inorganic & Nuclear ; Crystallography
语种英语
WOS记录号WOS:000232148100004
出版者CHINESE JOURNAL STRUCTURAL CHEMISTRY
URI标识http://www.irgrid.ac.cn/handle/1471x/2378047
专题中国科学院大学
通讯作者Hong, MC
作者单位1.Chinese Acad Sci, Fujian Inst Res Struct Matter, State Key Lab Struct Chem, Fujian 350002, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
推荐引用方式
GB/T 7714
Wang, RH,Gong, YQ,Han, L,et al. From chain to layer structure: zn-ii coordination polymers derived from diphenic acid[J]. Chinese journal of structural chemistry,2005,24(9):1007-1016.
APA Wang, RH,Gong, YQ,Han, L,Yuan, DQ,&Hong, MC.(2005).From chain to layer structure: zn-ii coordination polymers derived from diphenic acid.Chinese journal of structural chemistry,24(9),1007-1016.
MLA Wang, RH,et al."From chain to layer structure: zn-ii coordination polymers derived from diphenic acid".Chinese journal of structural chemistry 24.9(2005):1007-1016.

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来源:中国科学院大学

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