The synthesis and crystal structure of new 3,6-bis[1-(4-ethoxyphenyl)-5-methyl-1,2,3-triazol-4-yl]-s-triazolo[3,4-b]-1,3,4-thiadiazole
文献类型：期刊论文
| 作者 | Dong, HS; Wang, B |
| 刊名 | Journal of chemical crystallography
 |
| 出版日期 | 2005 |
| 卷号 | 35期号:1页码:61-65 |
| 关键词 | Crystal structure 1,2,3-triazole S-triazolo[3,4-b]-1,3,4-thiadiazole Synthesis |
| ISSN号 | 1074-1542 |
| DOI | 10.1007/s10870-005-1155-6 |
| 通讯作者 | Dong, hs(donghengshan@lzu.edu.cn) |
| 英文摘要 | The 3,6-bis[1-(4-ethoxyphenyl)-5-methyl-1,2,3-triazol-4-yl]-s-triazolo[3,4-b]-1,3,4-thiadiazole was synthesized from p-ethoxyaniline to 8 with 1-(4-ethoxyphenyl)-5-methyl- 1,2,3-triazol-4-caroxylic acid. the yielded product 9 was investigated with x-ray crystallographic, nmr, ms, and ir techniques. compound 9, c25h24n10o2s, mr = 528.60, crystallizes in the triclinic space group p (1) over bar with unit cell parameters a = 6.4490(10), b = 11.481(2) c = 18.168(4) angstrom, alpha = 72.08(3), beta = 86.57(3), gamma = 86.72(3)degrees. v = 1276.6(4) angstrom(3), z = 2, dx = 1.375 mgm(-3). the final r was 0.0589. |
| WOS关键词 | THIOSEMICARBAZIDES ; HETEROCYCLES |
| WOS研究方向 | Crystallography ; Spectroscopy |
| WOS类目 | Crystallography ; Spectroscopy |
| 语种 | 英语 |
| WOS记录号 | WOS:000227216600009 |
| 出版者 | SPRINGER/PLENUM PUBLISHERS |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2378245 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Dong, HS |
| 作者单位 | 1.Lanzhou Univ, Coll Chem & Chem Engn, Inst Organ Chem, Natl Lab Appl Organ Chem, Lanzhou 730000, Gansu, Peoples R China 2.Gansu Assoc Univ, Coll Sci & Engn, Lanzhou 730000, Gansu, Peoples R China |
| 推荐引用方式 GB/T 7714 | Dong, HS,Wang, B. The synthesis and crystal structure of new 3,6-bis[1-(4-ethoxyphenyl)-5-methyl-1,2,3-triazol-4-yl]-s-triazolo[3,4-b]-1,3,4-thiadiazole[J]. Journal of chemical crystallography,2005,35(1):61-65. |
| APA | Dong, HS,&Wang, B.(2005).The synthesis and crystal structure of new 3,6-bis[1-(4-ethoxyphenyl)-5-methyl-1,2,3-triazol-4-yl]-s-triazolo[3,4-b]-1,3,4-thiadiazole.Journal of chemical crystallography,35(1),61-65. |
| MLA | Dong, HS,et al."The synthesis and crystal structure of new 3,6-bis[1-(4-ethoxyphenyl)-5-methyl-1,2,3-triazol-4-yl]-s-triazolo[3,4-b]-1,3,4-thiadiazole".Journal of chemical crystallography 35.1(2005):61-65. |
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来源：中国科学院大学
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