Determination of manadione sodium bifulfite in injection with capillary electrophoresis
文献类型：期刊论文
| 作者 | Tang, YJ; Wu, MJ |
| 刊名 | Chinese journal of analytical chemistry
 |
| 出版日期 | 2005-06-01 |
| 卷号 | 33期号:6页码:828-830 |
| 关键词 | Capillary electrophoresis Menadione sodium bifulfite Sodium dodecylsulfate |
| ISSN号 | 0253-3820 |
| 通讯作者 | Wu, mj() |
| 英文摘要 | A method of determining menadione sodium bifulfite by high performance capillary electrophoresis with ultraviolet detection was developed. menadione sodium bifulfite was detected under the following separation conditions: uncoated fused silica capillary (55 cm x 75 mu m), background electrolyte 40 mmol/l phosphate +50 mmol/l sodium dodecylsulfate (sds) (ph=7.5), operation voltage 15 kv and ultraviolet detection wavelength 231 nm. the choices of the buffer and the ph value were discussed. especially, the mechanism of sds on the solubility enhancement was investigated in detail. the experimental results show that menadione sodium bifulfite in injection was quantified with pyridoxal 5-phosphate as the internal standard, which means that the determination of menadione sodium bifulfite was very simple, feasible and satisfactory. |
| WOS关键词 | MENADIONE ; BISULFITE |
| WOS研究方向 | Chemistry |
| WOS类目 | Chemistry, Analytical |
| 语种 | 英语 |
| WOS记录号 | WOS:000230362500022 |
| 出版者 | SCIENCE PRESS |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2378294 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Wu, MJ |
| 作者单位 | 1.Chinese Acad Sci, Changchun Inst Appl Chem, Natl Anal Res Ctr Electrochem & Spectroscopy, Changchun 130022, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China |
| 推荐引用方式 GB/T 7714 | Tang, YJ,Wu, MJ. Determination of manadione sodium bifulfite in injection with capillary electrophoresis[J]. Chinese journal of analytical chemistry,2005,33(6):828-830. |
| APA | Tang, YJ,&Wu, MJ.(2005).Determination of manadione sodium bifulfite in injection with capillary electrophoresis.Chinese journal of analytical chemistry,33(6),828-830. |
| MLA | Tang, YJ,et al."Determination of manadione sodium bifulfite in injection with capillary electrophoresis".Chinese journal of analytical chemistry 33.6(2005):828-830. |
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来源：中国科学院大学
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