The characterization of the intermediate produced in the synthesis of 1, 5-naphthalene dicarbamate by dimethylcarbonate method
文献类型：期刊论文
| 作者 | Xiao, FK; Zhang, DS; Dong, QN; Wei, W; Piao, ZS; Xu, H; Zhao, N; Sun, YH |
| 刊名 | Chinese journal of analytical chemistry
 |
| 出版日期 | 2006-03-01 |
| 卷号 | 34期号:3页码:415-417 |
| 关键词 | 5-amino-naphthalene-1-carbamate Structure characterization Mass spectrometry Fourier transform infrared Nuclear magnetic resonance |
| ISSN号 | 0253-3820 |
| 通讯作者 | Sun, yh() |
| 英文摘要 | It was found that the reaction of 1,5-naphthalene diamine (nda) with dimethylcarbonate (dmc) to produce 1,5-naphthalene dicarbamate was a series reaction through an intermediate. the intermediate was purified through extraction and crystallization and characterized by mass spectra, element analysis, fourier transform infrared spectra and h-1 nuclear magnetic resonance spectroscopy, the result indicats that the intermediate of the reaction is 5-amino-napbthalene-1-carbamate (anc) with a molecular weight of 216 and a composing of c12h12n2o2. |
| WOS研究方向 | Chemistry |
| WOS类目 | Chemistry, Analytical |
| 语种 | 英语 |
| WOS记录号 | WOS:000236528300034 |
| 出版者 | SCIENCE PRESS |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2379264 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Sun, YH |
| 作者单位 | 1.Chinese Acad Sci, Inst Coal Chem, State Key Lab Coal Convers, Taiyuan 030001, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China 3.Res Inst Jilin Petrochem Co Petrochina, Jilin 132021, Peoples R China |
| 推荐引用方式 GB/T 7714 | Xiao, FK,Zhang, DS,Dong, QN,et al. The characterization of the intermediate produced in the synthesis of 1, 5-naphthalene dicarbamate by dimethylcarbonate method[J]. Chinese journal of analytical chemistry,2006,34(3):415-417. |
| APA | Xiao, FK.,Zhang, DS.,Dong, QN.,Wei, W.,Piao, ZS.,...&Sun, YH.(2006).The characterization of the intermediate produced in the synthesis of 1, 5-naphthalene dicarbamate by dimethylcarbonate method.Chinese journal of analytical chemistry,34(3),415-417. |
| MLA | Xiao, FK,et al."The characterization of the intermediate produced in the synthesis of 1, 5-naphthalene dicarbamate by dimethylcarbonate method".Chinese journal of analytical chemistry 34.3(2006):415-417. |
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来源：中国科学院大学
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