Characterization of the intermediate and product in the synthesis of methyl-4,4'-di(phenylcarbamate) from the reaction of 4,4'-methylenedianiline with dimethyl carbonate
文献类型：期刊论文
| 作者 | Guo Xing-Cui1,2; Qin Zhang-Feng1; Wang Guo-Fu1; Dong Mei1; Zhao Rui-Hua1; Wang Jian-Guo1 |
| 刊名 | Chinese journal of analytical chemistry
 |
| 出版日期 | 2007-11-01 |
| 卷号 | 35期号:11页码:1625-1628 |
| 关键词 | Methyl-4,4'-di(phenylcarbamate) Methyl-4-4'-diphenylcarbamate Methyl-4-(4'-aminobenzyl) phenylcarbamate Mass spectrometry Fourier transform infrared Nuclear magnetic resonance |
| ISSN号 | 0253-3820 |
| 通讯作者 | Wang jian-guo(jccjgw@sxice.ac.cn) |
| 英文摘要 | The synthesis of methyl-4,4'-di(phenylcarbamate) (mdc) from the reaction of 4,4'-methylenedianiline (mda) with dimethylcarbonate (dmc) was investigated; the reaction intermediate and final product were separated, purified, analyzed and identified by liquid chromatography, mass spectrometry, element analysis, fourier transform infrared spectroscopy and h-1 nuclear magnetic resonance spectroscopy. the results illustrated that this synthesis reaction is a consecutive process through an intermediate; the final product is mdc and the intermediate is methyl-4-(4'-aminobenzyl) phenylcarbamate. |
| WOS关键词 | AROMATIC DIAMINES |
| WOS研究方向 | Chemistry |
| WOS类目 | Chemistry, Analytical |
| 语种 | 英语 |
| WOS记录号 | WOS:000252811700016 |
| 出版者 | SCIENCE CHINA PRESS |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2380455 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Wang Jian-Guo |
| 作者单位 | 1.Chinese Acad Sci, Inst Coal Chem, State Key Lab Coal Conversat, Taiyuan 030001, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China |
| 推荐引用方式 GB/T 7714 | Guo Xing-Cui,Qin Zhang-Feng,Wang Guo-Fu,et al. Characterization of the intermediate and product in the synthesis of methyl-4,4'-di(phenylcarbamate) from the reaction of 4,4'-methylenedianiline with dimethyl carbonate[J]. Chinese journal of analytical chemistry,2007,35(11):1625-1628. |
| APA | Guo Xing-Cui,Qin Zhang-Feng,Wang Guo-Fu,Dong Mei,Zhao Rui-Hua,&Wang Jian-Guo.(2007).Characterization of the intermediate and product in the synthesis of methyl-4,4'-di(phenylcarbamate) from the reaction of 4,4'-methylenedianiline with dimethyl carbonate.Chinese journal of analytical chemistry,35(11),1625-1628. |
| MLA | Guo Xing-Cui,et al."Characterization of the intermediate and product in the synthesis of methyl-4,4'-di(phenylcarbamate) from the reaction of 4,4'-methylenedianiline with dimethyl carbonate".Chinese journal of analytical chemistry 35.11(2007):1625-1628. |
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来源：中国科学院大学
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