Separation and determination of water soluble active components in salvia miltiorrhiza bunge and its pharmaceutical preparations by capillary zone electrophoresis with diode array detection
文献类型：期刊论文
| 作者 | Qiao, Chengdong; Zhao, Liang; Jiang, Shengxiang; Song, Pingshun |
| 刊名 | Journal of liquid chromatography & related technologies
 |
| 出版日期 | 2007 |
| 卷号 | 30期号:19页码:2819-2833 |
| 关键词 | Capillary zone electrophoresis Danshensu Separation Pharmaceutical preparations |
| ISSN号 | 1082-6076 |
| DOI | 10.1080/10826070701588513 |
| 通讯作者 | Jiang, shengxiang(qcdwh@yahoo.com.cn) |
| 英文摘要 | A novel, simple, and rapid method is developed for separating water soluble active components in salvia miltiorrhiza bunge and its pharmaceutical preparations by capillary zone electrophoresis with a diode array detector within 11 min under the optimal conditions. the repeatability (defined as relative standard deviation, rsd) was less than 4.45% with peak area evaluation and 2.13% with migration time evaluation. regression equations revealed linear relationships (r: 0.9964-0.9987) between the peak area of each analyte and the concentration. the detection limits (s/n = 3) of protocatechuic aldehyde, danshensu, and protocatechuic acid were 0.46, 0.62, and 0.28 mu g/ml, respectively. the proposed method has been satisfactorily applied to the analysis of water soluble active components in salvia miltiorrhiza bunge and its pharmaceutical preparations with recoveries in the range of 94%-101%. |
| WOS关键词 | PROTOCATECHUIC ALDEHYDE ; INTIMAL HYPERPLASIA ; RATS ; ANTIOXIDANT ; TANSHINONE ; DANSHEN ; CELLS ; ACID ; HPLC ; REDUCTION |
| WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
| WOS类目 | Biochemical Research Methods ; Chemistry, Analytical |
| 语种 | 英语 |
| WOS记录号 | WOS:000250551600002 |
| 出版者 | TAYLOR & FRANCIS INC |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2381181 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Jiang, Shengxiang |
| 作者单位 | 1.Chinese Acad Sci, Lanzhou Inst Chem Phys, Key Lab Nat Med Gansu Prov, Lanzhou 730000, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing, Peoples R China |
| 推荐引用方式 GB/T 7714 | Qiao, Chengdong,Zhao, Liang,Jiang, Shengxiang,et al. Separation and determination of water soluble active components in salvia miltiorrhiza bunge and its pharmaceutical preparations by capillary zone electrophoresis with diode array detection[J]. Journal of liquid chromatography & related technologies,2007,30(19):2819-2833. |
| APA | Qiao, Chengdong,Zhao, Liang,Jiang, Shengxiang,&Song, Pingshun.(2007).Separation and determination of water soluble active components in salvia miltiorrhiza bunge and its pharmaceutical preparations by capillary zone electrophoresis with diode array detection.Journal of liquid chromatography & related technologies,30(19),2819-2833. |
| MLA | Qiao, Chengdong,et al."Separation and determination of water soluble active components in salvia miltiorrhiza bunge and its pharmaceutical preparations by capillary zone electrophoresis with diode array detection".Journal of liquid chromatography & related technologies 30.19(2007):2819-2833. |
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来源：中国科学院大学
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