Hydrothermal synthesis and characterization of linbo3 crystal
文献类型：期刊论文
| 作者 | Yu, Ji; Liu, Xingquan |
| 刊名 | Materials letters
 |
| 出版日期 | 2007 |
| 卷号 | 61期号:2页码:355-358 |
| 关键词 | Linbo3 Hydrothermal synthesis Xrd Ft-ir Sem |
| ISSN号 | 0167-577X |
| DOI | 10.1016/j.matlet.2006.04.087 |
| 通讯作者 | Liu, xingquan(lxquan2000@hotmail.com) |
| 英文摘要 | Lithium mobate crystal was successfully synthesized via hydrothermal synthesis method using lioh center dot h2o or lino3 and nb2o5 as starting materials in water or ammonia solution. x-ray diffraction (xrd), fourier-transform infrared (ft-ir) spectra and scanning electron microscopy (sem) were used to characterize the as-prepared samples. the synthesis conditions such as crystallization temperature and time as well as ammonia concentration (when using lino3 as li source) were investigated. the results demonstrate that the crystallization and purity of the as-prepared samples were increased with the increase of time when temperature was at 260 degrees c. when using lino3 as li source a basic solution was necessary to synthesize linbo3. in the present work ammonia solution was used instead of water to obtain alkalescence solvent. xrd results revealed that the as-prepared samples had a hexagonal structure. ft-ir results displayed that the linbo3 phase could be completely formed and no secondary phase was found under proper conditions. sem picture showed that the morphology of the sample was more perfect and bigger with increasing reaction time. (c) 2006 elsevier b.v. all rights reserved. |
| WOS关键词 | LIQUID-PHASE EPITAXY ; THIN-FILMS ; LITHIUM-NIOBATE ; OPTICAL-PROPERTIES ; GROWTH ; PRECURSOR |
| WOS研究方向 | Materials Science ; Physics |
| WOS类目 | Materials Science, Multidisciplinary ; Physics, Applied |
| 语种 | 英语 |
| WOS记录号 | WOS:000243253800013 |
| 出版者 | ELSEVIER SCIENCE BV |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2382266 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Liu, Xingquan |
| 作者单位 | 1.Chinese Acad Sci, Chengdu Inst Organ Chem, Chengdu 610041, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China |
| 推荐引用方式 GB/T 7714 | Yu, Ji,Liu, Xingquan. Hydrothermal synthesis and characterization of linbo3 crystal[J]. Materials letters,2007,61(2):355-358. |
| APA | Yu, Ji,&Liu, Xingquan.(2007).Hydrothermal synthesis and characterization of linbo3 crystal.Materials letters,61(2),355-358. |
| MLA | Yu, Ji,et al."Hydrothermal synthesis and characterization of linbo3 crystal".Materials letters 61.2(2007):355-358. |
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来源：中国科学院大学
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