The isolation of 1,2,3,4,6-penta-o-galloyl-beta-d-glucose from acer truncatum bunge by high-speed counter-current chromatography
文献类型：期刊论文
| 作者 | Zhao, Wen-Hua; Gao, Chun-Chun; Ma, Xiao-Feng; Bai, Xiao-Yu; Zhang, Ying-Xia |
| 刊名 | Journal of chromatography b-analytical technologies in the biomedical and life sciences
 |
| 出版日期 | 2007-05-01 |
| 卷号 | 850期号:1-2页码:523-527 |
| 关键词 | 1,2,3,4,6-penta-o-galloyl-beta-d-glucose Acer truncatum bunge Counter-current chromatography |
| ISSN号 | 1570-0232 |
| DOI | 10.1016/j.jchromb.2006.11.002 |
| 通讯作者 | Zhang, ying-xia(zwhua@ccmu.edu.cn) |
| 英文摘要 | High-speed counter-current chromatography (hsccc) was successfully used for the isolation and purification of 1,2,3,4,6-penta-o-galloyl-beta-d-glucose from the ethyl acetate extract of the leaves of acer truncatum bunge using a two-phase system composed of n-hexane-ethyl acetate-methanol-water at a volume ratio of (0.25:5:1:5, v/v/v/v) for the first time. each injection of 80 mg crude extract yielded 7.25 mg of pure 1,2,3,4,6-penta-o-galloyl-beta-d-glucose. high-performance liquid chromatography (hplc) analyses of the ccc fraction revealed that the purity of 1,2,3,4,6-penta-o-galloyl-beta-d-glucose was over 95%. (c) 2006 elsevier b.v. all rights reserved. |
| WOS关键词 | PREPARATIVE ISOLATION ; PURIFICATION ; SEPARATION ; EXTRACT ; CELLS ; ISOFLAVONES ; POLYPHENOLS ; INHIBITION ; INDUCTION ; ALKALOIDS |
| WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
| WOS类目 | Biochemical Research Methods ; Chemistry, Analytical |
| 语种 | 英语 |
| WOS记录号 | WOS:000246703500067 |
| 出版者 | ELSEVIER SCIENCE BV |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2382385 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Zhang, Ying-Xia |
| 作者单位 | 1.Capital Med Univ, Dept Biol Chem, Beijing 100069, Peoples R China 2.Harbin Commercial Univ, Dept Pharm, Harbin 150076, Peoples R China 3.Grad Univ, Chinese Acad Sci, Dept Biol, Beijing 100049, Peoples R China 4.Capital Med Univ, Lab Liver Protect & Regulat, Beijing 100069, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhao, Wen-Hua,Gao, Chun-Chun,Ma, Xiao-Feng,et al. The isolation of 1,2,3,4,6-penta-o-galloyl-beta-d-glucose from acer truncatum bunge by high-speed counter-current chromatography[J]. Journal of chromatography b-analytical technologies in the biomedical and life sciences,2007,850(1-2):523-527. |
| APA | Zhao, Wen-Hua,Gao, Chun-Chun,Ma, Xiao-Feng,Bai, Xiao-Yu,&Zhang, Ying-Xia.(2007).The isolation of 1,2,3,4,6-penta-o-galloyl-beta-d-glucose from acer truncatum bunge by high-speed counter-current chromatography.Journal of chromatography b-analytical technologies in the biomedical and life sciences,850(1-2),523-527. |
| MLA | Zhao, Wen-Hua,et al."The isolation of 1,2,3,4,6-penta-o-galloyl-beta-d-glucose from acer truncatum bunge by high-speed counter-current chromatography".Journal of chromatography b-analytical technologies in the biomedical and life sciences 850.1-2(2007):523-527. |
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