Preparation of new hybrid organic/inorganic polymeric chiral stationary phases for ligand-exchange chromatography
文献类型：期刊论文
| 作者 | Song, Rui Juan; Fu, Yu; Yao, Na; De Long, Yuan; Huang, Tian Bao |
| 刊名 | Chinese chemical letters
 |
| 出版日期 | 2007-10-01 |
| 卷号 | 18期号:10页码:1250-1252 |
| 关键词 | Chiral stationary phase Ligand-exchange chromatography Dl-hydroxyl acid Surface grafting Dl-amino acid |
| ISSN号 | 1001-8417 |
| DOI | 10.1016/j.celet.2007.07.022 |
| 通讯作者 | Huang, tian bao(tbhuang@cioc.ac.cn) |
| 英文摘要 | Three new hybrid organic/inorganic polymeric ligand-exchange chiral stationary phases were developed by radical chain transfer reaction and surface grafting on silica gel, and successfully used for the enantioseparations of dl-amino acids and dl-hydroxyl acids. the resolutions were achieved by using water containing 2.0 x 10(-4) mol/l of cuac2 as a mobile phase, column temperature of 40 degrees c, flow rate of 1.0 ml/min and detection at uv 254 nm. the elution order of d-isorner before l-isomer was observed for all dl-amino acids resolved except dl-pro. (c) 2007 tian bao huang. published by elsevier b.v. on behalf of chinese chemical society. all rights reserved. |
| WOS关键词 | SEPARATION ; SILICA |
| WOS研究方向 | Chemistry |
| WOS类目 | Chemistry, Multidisciplinary |
| 语种 | 英语 |
| WOS记录号 | WOS:000250494100025 |
| 出版者 | CHINESE CHEMICAL SOC |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2382741 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Huang, Tian Bao |
| 作者单位 | 1.Chinese Acad Sci, Chengdu Inst Organ Chem, Chengdu 610041, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China |
| 推荐引用方式 GB/T 7714 | Song, Rui Juan,Fu, Yu,Yao, Na,et al. Preparation of new hybrid organic/inorganic polymeric chiral stationary phases for ligand-exchange chromatography[J]. Chinese chemical letters,2007,18(10):1250-1252. |
| APA | Song, Rui Juan,Fu, Yu,Yao, Na,De Long, Yuan,&Huang, Tian Bao.(2007).Preparation of new hybrid organic/inorganic polymeric chiral stationary phases for ligand-exchange chromatography.Chinese chemical letters,18(10),1250-1252. |
| MLA | Song, Rui Juan,et al."Preparation of new hybrid organic/inorganic polymeric chiral stationary phases for ligand-exchange chromatography".Chinese chemical letters 18.10(2007):1250-1252. |
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来源：中国科学院大学
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