Enantiomeric resolution of tebuconazole on immobilized cellulose chiral stationary phase
文献类型：期刊论文
| 作者 | Ming Yong-Fei; Zhao Liang; Zhang Hong-Li; Shi Yan-Ping; Li Yong-Min |
| 刊名 | Chemical journal of chinese universities-chinese
 |
| 出版日期 | 2007-02-10 |
| 卷号 | 28期号:2页码:258-260 |
| 关键词 | Immobilization Chiral stationary phase Chiral resolution Tebuconazole |
| ISSN号 | 0251-0790 |
| 通讯作者 | Li yong-min(zhaol@ns.lzb.ac.cn) |
| 英文摘要 | The chiral stationary pahse of 3,5-dimethylphenylcarbamates of cellulose chemically bonded to 3-aminopropyl silica gel at the 6-position of the glucose units was prepared. the racemates of tebuconazole were resolved on the new immobilized chiral stationary phase, and the influences of modifiers(alcohols, thf and chloroform) in the mobile phase on the resolution were investigated. the chromatographic conditions were optimized. the results show that the new immobilized chiral stationary phase exhibits a good stereoselectivity to tebuconzole. the best resolution of 1.51 of tebuconazole was obtained by using hexane/2-propanol/thf (volume ratio 90: 5: 5) as the mobile phase on a 150 min column. |
| WOS关键词 | PERFORMANCE LIQUID-CHROMATOGRAPHY ; SILICA-GEL |
| WOS研究方向 | Chemistry |
| WOS类目 | Chemistry, Multidisciplinary |
| 语种 | 英语 |
| WOS记录号 | WOS:000244413000015 |
| 出版者 | HIGHER EDUCATION PRESS |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2383908 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Li Yong-Min |
| 作者单位 | 1.Chinese Acad Sci, Lanzhou Inst Chem Phys, Key Lab Nat Med Gansu Prov, Lanzhou 730000, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China |
| 推荐引用方式 GB/T 7714 | Ming Yong-Fei,Zhao Liang,Zhang Hong-Li,et al. Enantiomeric resolution of tebuconazole on immobilized cellulose chiral stationary phase[J]. Chemical journal of chinese universities-chinese,2007,28(2):258-260. |
| APA | Ming Yong-Fei,Zhao Liang,Zhang Hong-Li,Shi Yan-Ping,&Li Yong-Min.(2007).Enantiomeric resolution of tebuconazole on immobilized cellulose chiral stationary phase.Chemical journal of chinese universities-chinese,28(2),258-260. |
| MLA | Ming Yong-Fei,et al."Enantiomeric resolution of tebuconazole on immobilized cellulose chiral stationary phase".Chemical journal of chinese universities-chinese 28.2(2007):258-260. |
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来源：中国科学院大学
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