Highly uniform and monodisperse ba(2)cif(3) microrods: solvothermal synthesis and characterization
文献类型:期刊论文
作者 | Zhang, Xiaoming; Li, Chunxia; Zhang, Cuimiao; Yang, Jun; Quan, Zewei; Yang, Piaoping; Lin, Jun1 |
刊名 | Crystal growth & design
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出版日期 | 2008-12-01 |
卷号 | 8期号:12页码:4564-4570 |
ISSN号 | 1528-7483 |
DOI | 10.1021/cg800619z |
通讯作者 | Lin, jun(jlin@ciac.jl.cn) |
英文摘要 | One-dimensional hexagonal ba(2)cif(3) microrods with highly uniform morphology and size have been successfully synthesized via a facile solvothermal method at a low temperature (160 degrees c). x-ray diffraction (xrd), scanning electron microscopy (sem), and transmission electron microscopy (tem) were used to characterize the samples. the synthesis process, based on a phase-transfer and separation mechanism, allows the control of properties such as particle size and shape in low dispersity by bonding the surfactant oleic acid to the crystal surface. we propose a possible formation process and preliminary growth mechanism for the microrods based on the effect of oleic acid. in the synthetic process, oleic acid as a surfactant plays a crucial role in confining the growth of the ba(2)cif(3) microcrystals. under different reaction conditions, ba(2)cif(3) microcrystals with different shapes and sizes can be obtained. |
WOS关键词 | COLLOIDAL SEMICONDUCTOR NANOCRYSTALS ; ONE-DIMENSIONAL NANOSTRUCTURES ; EARTH FLUORIDE NANOCRYSTALS ; HYDROTHERMAL SYNTHESIS ; SHAPE-CONTROL ; OPTICAL-PROPERTIES ; GENERAL-SYNTHESIS ; ZINC OXIDE ; NANOPARTICLES ; NANOWIRES |
WOS研究方向 | Chemistry ; Crystallography ; Materials Science |
WOS类目 | Chemistry, Multidisciplinary ; Crystallography ; Materials Science, Multidisciplinary |
语种 | 英语 |
WOS记录号 | WOS:000261379400059 |
出版者 | AMER CHEMICAL SOC |
URI标识 | http://www.irgrid.ac.cn/handle/1471x/2386295 |
专题 | 中国科学院大学 |
通讯作者 | Lin, Jun |
作者单位 | 1.Chinese Acad Sci, Changchun Inst Appl Chem, State Key Lab Rare Earth Resource Utilizat, Changchun 130022, Peoples R China 2.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China |
推荐引用方式 GB/T 7714 | Zhang, Xiaoming,Li, Chunxia,Zhang, Cuimiao,et al. Highly uniform and monodisperse ba(2)cif(3) microrods: solvothermal synthesis and characterization[J]. Crystal growth & design,2008,8(12):4564-4570. |
APA | Zhang, Xiaoming.,Li, Chunxia.,Zhang, Cuimiao.,Yang, Jun.,Quan, Zewei.,...&Lin, Jun.(2008).Highly uniform and monodisperse ba(2)cif(3) microrods: solvothermal synthesis and characterization.Crystal growth & design,8(12),4564-4570. |
MLA | Zhang, Xiaoming,et al."Highly uniform and monodisperse ba(2)cif(3) microrods: solvothermal synthesis and characterization".Crystal growth & design 8.12(2008):4564-4570. |
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来源:中国科学院大学
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