Novel reversed-phase high-performance liquid chromatography stationary phase with oligo(ethylene glycol) "click" to silica
文献类型:期刊论文
作者 | Guo, Zhimou1; Liu, Yanfang1; Xu, Junyan1,2; Xu, Qing1; Xue, Xingya1; Zhang, Feifang1; Ke, Yanxiong1,2; Liang, Xinmiao1,2; Lei, Aiwen3 |
刊名 | Journal of chromatography a
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出版日期 | 2008-05-16 |
卷号 | 1191期号:1-2页码:78-82 |
关键词 | Oligo(ethylene glycol) Stationary phase Click chemistry High-performance liquid chromatography |
ISSN号 | 0021-9673 |
DOI | 10.1016/j.chroma.2007.11.093 |
通讯作者 | Liang, xinmiao(liangxm@dicp.ac.cn) |
英文摘要 | Oligo(ethylene glycol) (oeg) covalently bonded silica was prepared by using click chemistry and employed as a stationary phase for reversed-phase high-performance liquid chromatography. the column efficiency and effect of organic modifier content on retention were investigated. the separation selectivity was also studied with phenyl compounds and an actual sample of natural products. the results indicated that the stationary phase possessed good separation efficiency and separation selectivity in r-p-hplc mode. moreover, the stationary phase showed good complementary separation selectivity to the c18 stationary phase. the oeg stationary phase had "clustering" function for "homologous component" in the separation of natural products. (c) 2007 elsevier b.v. all rights reserved. |
WOS关键词 | EMBEDDED UREA GROUPS ; SELF-ASSEMBLED MONOLAYERS ; BONDED CALIXARENES ; RP-HPLC ; SEPARATION ; CHEMISTRY ; SURFACES ; SELECTIVITY ; RETENTION ; IONS |
WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
WOS类目 | Biochemical Research Methods ; Chemistry, Analytical |
语种 | 英语 |
WOS记录号 | WOS:000256326400008 |
出版者 | ELSEVIER SCIENCE BV |
URI标识 | http://www.irgrid.ac.cn/handle/1471x/2387351 |
专题 | 中国科学院大学 |
通讯作者 | Liang, Xinmiao |
作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Grad Sch, Dalian 116023, Peoples R China 2.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China 3.Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Peoples R China |
推荐引用方式 GB/T 7714 | Guo, Zhimou,Liu, Yanfang,Xu, Junyan,et al. Novel reversed-phase high-performance liquid chromatography stationary phase with oligo(ethylene glycol) "click" to silica[J]. Journal of chromatography a,2008,1191(1-2):78-82. |
APA | Guo, Zhimou.,Liu, Yanfang.,Xu, Junyan.,Xu, Qing.,Xue, Xingya.,...&Lei, Aiwen.(2008).Novel reversed-phase high-performance liquid chromatography stationary phase with oligo(ethylene glycol) "click" to silica.Journal of chromatography a,1191(1-2),78-82. |
MLA | Guo, Zhimou,et al."Novel reversed-phase high-performance liquid chromatography stationary phase with oligo(ethylene glycol) "click" to silica".Journal of chromatography a 1191.1-2(2008):78-82. |
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来源:中国科学院大学
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