Chromatographic evaluation of octadecyl-bonded tio2/sio2 stationary phase with engelhardt and tanaka test mixtures
文献类型：期刊论文
| 作者 | Ge, Jin1,2; Zhao, Liang1; Shi, Yan-Ping1 |
| 刊名 | Journal of liquid chromatography & related technologies
 |
| 出版日期 | 2008 |
| 卷号 | 31期号:2页码:151-160 |
| 关键词 | Tio2/sio2 Rp-hplc Octadecyl-bonded stationary phase Basic compounds |
| ISSN号 | 1082-6076 |
| DOI | 10.1080/10826070701738696 |
| 通讯作者 | Shi, yan-ping(shiyp@lzb.ac.cn) |
| 英文摘要 | Chromatographic performance of octadecyl-bonded tio2/sio2 stationary phase was evaluated with engelhardt and tanaka test mixtures. in the two test protocol, some parameters influencing the retention, such as methylene selectivity (ch2), steric selectivity (o/t), hydrogen bonding capacity (c/p), and ion exchange capacity (b/p) were obtained. by separating several same compounds with different mobile phases, different results were obtained and they were compared with that in the reference, in which octadecyl-bonded titania packing was prepared and a similar test was carried out. all of the results suggest that the octadecyl-bonded tio2/sio2 stationary phase not only has good methylene selectivity and steric selectivity, but also shows a large potential in the separation of basic compounds. |
| WOS关键词 | PERFORMANCE LIQUID-CHROMATOGRAPHY ; REVERSED-PHASE ; RETENTION BEHAVIOR ; PACKING MATERIAL ; RP-HPLC ; TITANIA ; SUPPORTS ; SILICA |
| WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
| WOS类目 | Biochemical Research Methods ; Chemistry, Analytical |
| 语种 | 英语 |
| WOS记录号 | WOS:000252347800001 |
| 出版者 | TAYLOR & FRANCIS INC |
| URI标识 | http://www.irgrid.ac.cn/handle/1471x/2388257 |
| 专题 | 中国科学院大学 |
| 通讯作者 | Shi, Yan-Ping |
| 作者单位 | 1.Chinese Acad Sci, Lanzhou Inst Chem Phys, Key Lab Nat Med, Lanzhou 730000, Gansu, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing, Peoples R China |
| 推荐引用方式 GB/T 7714 | Ge, Jin,Zhao, Liang,Shi, Yan-Ping. Chromatographic evaluation of octadecyl-bonded tio2/sio2 stationary phase with engelhardt and tanaka test mixtures[J]. Journal of liquid chromatography & related technologies,2008,31(2):151-160. |
| APA | Ge, Jin,Zhao, Liang,&Shi, Yan-Ping.(2008).Chromatographic evaluation of octadecyl-bonded tio2/sio2 stationary phase with engelhardt and tanaka test mixtures.Journal of liquid chromatography & related technologies,31(2),151-160. |
| MLA | Ge, Jin,et al."Chromatographic evaluation of octadecyl-bonded tio2/sio2 stationary phase with engelhardt and tanaka test mixtures".Journal of liquid chromatography & related technologies 31.2(2008):151-160. |
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来源：中国科学院大学
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