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Systematic study of beta-asarone-rich volatile oil from acori graminei rhizoma by off-line supercritical co2 extraction-gas chromatography-mass spectrometry

文献类型:期刊论文

作者Dai, Jian1,2; Ha, Chengyong1; Shen, Minmin1
刊名Journal of separation science
出版日期2008-03-01
卷号31期号:4页码:714-720
关键词Acori graminei rhizoma Beta-asarone Gc-ms Supercritical fluid extraction Volatile oil
ISSN号1615-9306
DOI10.1002/jssc.200700242
通讯作者Ha, chengyong(cyha@gic.ac.cn)
英文摘要Supercritical co2 extraction (sce) technology was used to extract a volatile oil, rich in beta-asarone, from acori graminei rhizoma (agr). the effect of different extraction and fractionation parameters on oil yield and selectivity towards beta-asarone was investigated by sce using commercial agr samples. the optimal conditions (p-e/ t-e = 10 mpa/45 degrees c; p-f1/t-f1 = 8 mpa/-10 degrees c; p-f2/t-f1= 2 mpa/10 degrees c) gave a good oil yield and selectivity for beta-asarone. the extracts were also analyzed by gc-ms and compared with the volatile oil obtained by hydrodistillation, in which 39 main constituents including beta-asarone were found. different cultivated agr samples obtained from three areas of china were evaluated in terms of their volatile oil compositions obtained by extraction of commercial agr samples under optimal conditions; the extract of the guangdong (gd) sample showed a high beta-asarone content.
WOS关键词FLUID EXTRACTION ; CARBON-DIOXIDE ; FRACTIONATION ; SOLUBILITIES ; COMPONENT
WOS研究方向Chemistry
WOS类目Chemistry, Analytical
语种英语
WOS记录号WOS:000254137900015
出版者WILEY-V C H VERLAG GMBH
URI标识http://www.irgrid.ac.cn/handle/1471x/2390062
专题中国科学院大学
通讯作者Ha, Chengyong
作者单位1.Chinese Acad Sci, Guangzhou Inst Chem, Key Lab Cellulose & Lignocellulos Chem, Guangzhou 510650, Guangdong, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing, Peoples R China
推荐引用方式
GB/T 7714
Dai, Jian,Ha, Chengyong,Shen, Minmin. Systematic study of beta-asarone-rich volatile oil from acori graminei rhizoma by off-line supercritical co2 extraction-gas chromatography-mass spectrometry[J]. Journal of separation science,2008,31(4):714-720.
APA Dai, Jian,Ha, Chengyong,&Shen, Minmin.(2008).Systematic study of beta-asarone-rich volatile oil from acori graminei rhizoma by off-line supercritical co2 extraction-gas chromatography-mass spectrometry.Journal of separation science,31(4),714-720.
MLA Dai, Jian,et al."Systematic study of beta-asarone-rich volatile oil from acori graminei rhizoma by off-line supercritical co2 extraction-gas chromatography-mass spectrometry".Journal of separation science 31.4(2008):714-720.

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来源:中国科学院大学

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