Methanol-mediated solvothermal synthesis of hexagonal cds hollow nanospheres
文献类型:期刊论文
作者 | Zheng Lin-Lin1; Feng Shou-Ai2,3; Gao Feng1; Zhu Zhen-Ping2,3 |
刊名 | Journal of inorganic materials
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出版日期 | 2009 |
卷号 | 24期号:1页码:61-64 |
关键词 | Cds Hollow nanosphere Mathanol Solvothermal synthesis |
ISSN号 | 1000-324X |
通讯作者 | Zheng lin-lin(zhenglinlin_@163.com) |
英文摘要 | Cds hollow nanospheres were synthesized via solvothermal route from cadmium nitrate and thiourea with methanol as medium. morphology and structures of the as-obtained products were characterized by tem, eds and xrd. tem and eds analysis show that the products are mainly onion-like cds hollow nanospheres, with external diameter of 5 - 17nm and hollow inner size of 3 - 14nm. xrd tests indicate that these hollow nanospheres exhibit hexagonal wurtzite structure. the function of alcohol solvent oil the growth of cds nanostructure is also studied preliminary. as absolute ethanol or 1-pentanol is employed as a substitute for solvent, the products are congeries of cds nanoparticles and microspheres assembled by cds nanoparticles, respectively. the results demonstrate that methanol plays a significant role in the formation of hollow structure. the formation of hollow nanospheres may be caused by curling of cds nanoflakes under the high vapor pressure of methanol. |
WOS关键词 | TEMPLATE-INTERFACE REACTION ; SPHERES ; ASSEMBLIES ; ROUTE ; US |
WOS研究方向 | Materials Science |
WOS类目 | Materials Science, Ceramics |
语种 | 英语 |
WOS记录号 | WOS:000262534800013 |
出版者 | SCIENCE PRESS |
URI标识 | http://www.irgrid.ac.cn/handle/1471x/2399634 |
专题 | 中国科学院大学 |
通讯作者 | Zheng Lin-Lin |
作者单位 | 1.Taiyuan Univ Technol, Coll Mat Sci & Engn, Taiyuan 030024, Peoples R China 2.Chinese Acad Sci, Inst Coal Chem, State Key Lab Coal Convers, Taiyuan 030001, Peoples R China 3.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China |
推荐引用方式 GB/T 7714 | Zheng Lin-Lin,Feng Shou-Ai,Gao Feng,et al. Methanol-mediated solvothermal synthesis of hexagonal cds hollow nanospheres[J]. Journal of inorganic materials,2009,24(1):61-64. |
APA | Zheng Lin-Lin,Feng Shou-Ai,Gao Feng,&Zhu Zhen-Ping.(2009).Methanol-mediated solvothermal synthesis of hexagonal cds hollow nanospheres.Journal of inorganic materials,24(1),61-64. |
MLA | Zheng Lin-Lin,et al."Methanol-mediated solvothermal synthesis of hexagonal cds hollow nanospheres".Journal of inorganic materials 24.1(2009):61-64. |
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来源:中国科学院大学
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