Synthesis of ti3sic2 by high energy ball milling and reactive sintering from ti, si, and c elements
文献类型:期刊论文
作者 | Meng, Fanling1,2,3; Chaffron, Laurent1; Zhou, Yanchun3 |
刊名 | Journal of nuclear materials
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出版日期 | 2009-04-30 |
卷号 | 386-88页码:647-649 |
ISSN号 | 0022-3115 |
DOI | 10.1016/j.jnucmat.2008.12.321 |
通讯作者 | Chaffron, laurent(laurent.chaffron@cea.fr) |
英文摘要 | We present an original method of preparation of nanostructured ti3sic2 compound based on high energy ball milling and reactive sintering techniques. starting materials are ti, si, and c elements. x-ray diffraction and secondary electron microscopy are used to identify the formed phases and to analyze the obtained microstructures. lower milling intensity and shorter milling time are found as the best milling conditions in order to get an intimate mixture of the three elements without formation of detectable secondary phases. the optimized sintering temperature is equal to 1350 degrees c. a method used for minimizing the oxygen content in the final compound is presented. (c) 2008 elsevier b.v. all rights reserved. |
WOS关键词 | POWDER SYNTHESIS ; CARBIDE ; FABRICATION ; MIXTURES ; CERAMICS ; PHASES |
WOS研究方向 | Materials Science ; Nuclear Science & Technology ; Mining & Mineral Processing |
WOS类目 | Materials Science, Multidisciplinary ; Nuclear Science & Technology ; Mining & Mineral Processing |
语种 | 英语 |
WOS记录号 | WOS:000266386900161 |
出版者 | ELSEVIER SCIENCE BV |
URI标识 | http://www.irgrid.ac.cn/handle/1471x/2403647 |
专题 | 中国科学院大学 |
通讯作者 | Chaffron, Laurent |
作者单位 | 1.CEA Saclay, DENDANS, DMN, SRMP,SRMA,LTMEX, F-91191 Gif Sur Yvette, France 2.Chinese Acad Sci, Grad Sch, Inst Met Res, Shenyang Natl Lab Mat Sci, Beijing 100039, Peoples R China 3.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China |
推荐引用方式 GB/T 7714 | Meng, Fanling,Chaffron, Laurent,Zhou, Yanchun. Synthesis of ti3sic2 by high energy ball milling and reactive sintering from ti, si, and c elements[J]. Journal of nuclear materials,2009,386-88:647-649. |
APA | Meng, Fanling,Chaffron, Laurent,&Zhou, Yanchun.(2009).Synthesis of ti3sic2 by high energy ball milling and reactive sintering from ti, si, and c elements.Journal of nuclear materials,386-88,647-649. |
MLA | Meng, Fanling,et al."Synthesis of ti3sic2 by high energy ball milling and reactive sintering from ti, si, and c elements".Journal of nuclear materials 386-88(2009):647-649. |
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来源:中国科学院大学
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