中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Purification of single-walled carbon nanotubes by oxygen oxidation in licl-kcl molten salt

文献类型:期刊论文

作者Qu Meizhen1,2; Lin Haoqiang1; Yu Zuolong1
刊名Acta chimica sinica
出版日期2010-03-14
卷号68期号:5页码:413-417
关键词Carbon nanotube Molten salt Amorphous carbon Oxygen oxidation
ISSN号0567-7351
通讯作者Qu meizhen(mzhqu@cioc.ac.cn)
英文摘要The purification of swcnt by oxygen oxidation in licl-kcl molten salt was investigated. 5 g of as-prepared swcnt was suspended in 200 g of molten salt (w(licl) : w(kcl) = 55 : 45) at 470 degrees c by agitation. after 2 h oxidation in 300 ml.min(-1) oxygen flow, 3.8% of purified swcnt was obtained. the oxidation degree could be controlled by adjusting the reaction temperature and oxygen flow rate. scanning electron microscopy (sem), transmission electron microscopy (tem), thermogravimetric analysis (tga) and raman spectra were employed to characterize the as-prepared and purified swcnt. the results indicated that almost all of the amorphous carbon in as-prepared swcnt was removed. however, the swcnt can survive from this purification process.
WOS关键词CATALYST
WOS研究方向Chemistry
WOS类目Chemistry, Multidisciplinary
语种英语
WOS记录号WOS:000275970300007
出版者SCIENCE PRESS
URI标识http://www.irgrid.ac.cn/handle/1471x/2405910
专题中国科学院大学
通讯作者Qu Meizhen
作者单位1.Chinese Acad Sci, Chengdu Inst Organ Chem, Chengdu 610041, Peoples R China
2.Chinese Acad Sci, Grad Univ, Beijing 100039, Peoples R China
推荐引用方式
GB/T 7714
Qu Meizhen,Lin Haoqiang,Yu Zuolong. Purification of single-walled carbon nanotubes by oxygen oxidation in licl-kcl molten salt[J]. Acta chimica sinica,2010,68(5):413-417.
APA Qu Meizhen,Lin Haoqiang,&Yu Zuolong.(2010).Purification of single-walled carbon nanotubes by oxygen oxidation in licl-kcl molten salt.Acta chimica sinica,68(5),413-417.
MLA Qu Meizhen,et al."Purification of single-walled carbon nanotubes by oxygen oxidation in licl-kcl molten salt".Acta chimica sinica 68.5(2010):413-417.

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来源:中国科学院大学

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