Purification of single-walled carbon nanotubes by oxygen oxidation in licl-kcl molten salt
文献类型:期刊论文
作者 | Qu Meizhen1,2; Lin Haoqiang1; Yu Zuolong1 |
刊名 | Acta chimica sinica
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出版日期 | 2010-03-14 |
卷号 | 68期号:5页码:413-417 |
关键词 | Carbon nanotube Molten salt Amorphous carbon Oxygen oxidation |
ISSN号 | 0567-7351 |
通讯作者 | Qu meizhen(mzhqu@cioc.ac.cn) |
英文摘要 | The purification of swcnt by oxygen oxidation in licl-kcl molten salt was investigated. 5 g of as-prepared swcnt was suspended in 200 g of molten salt (w(licl) : w(kcl) = 55 : 45) at 470 degrees c by agitation. after 2 h oxidation in 300 ml.min(-1) oxygen flow, 3.8% of purified swcnt was obtained. the oxidation degree could be controlled by adjusting the reaction temperature and oxygen flow rate. scanning electron microscopy (sem), transmission electron microscopy (tem), thermogravimetric analysis (tga) and raman spectra were employed to characterize the as-prepared and purified swcnt. the results indicated that almost all of the amorphous carbon in as-prepared swcnt was removed. however, the swcnt can survive from this purification process. |
WOS关键词 | CATALYST |
WOS研究方向 | Chemistry |
WOS类目 | Chemistry, Multidisciplinary |
语种 | 英语 |
WOS记录号 | WOS:000275970300007 |
出版者 | SCIENCE PRESS |
URI标识 | http://www.irgrid.ac.cn/handle/1471x/2405910 |
专题 | 中国科学院大学 |
通讯作者 | Qu Meizhen |
作者单位 | 1.Chinese Acad Sci, Chengdu Inst Organ Chem, Chengdu 610041, Peoples R China 2.Chinese Acad Sci, Grad Univ, Beijing 100039, Peoples R China |
推荐引用方式 GB/T 7714 | Qu Meizhen,Lin Haoqiang,Yu Zuolong. Purification of single-walled carbon nanotubes by oxygen oxidation in licl-kcl molten salt[J]. Acta chimica sinica,2010,68(5):413-417. |
APA | Qu Meizhen,Lin Haoqiang,&Yu Zuolong.(2010).Purification of single-walled carbon nanotubes by oxygen oxidation in licl-kcl molten salt.Acta chimica sinica,68(5),413-417. |
MLA | Qu Meizhen,et al."Purification of single-walled carbon nanotubes by oxygen oxidation in licl-kcl molten salt".Acta chimica sinica 68.5(2010):413-417. |
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来源:中国科学院大学
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