Synthesis and crystal structure of a new tetracopper complex [cu(h2o)(3)cu(hcdta)](2)(clo4)(2)center dot h2o
文献类型:期刊论文
作者 | Wang Mei-Xiang1,2; Dang Zhen-Hua1,2; Xu Li1 |
刊名 | Chinese journal of structural chemistry
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出版日期 | 2010 |
卷号 | 29期号:4页码:551-554 |
关键词 | Copper Supramolecular Two-dimensional Weak interaction |
ISSN号 | 0254-5861 |
通讯作者 | Xu li(xli@ms.fjirsm.ac.cn) |
英文摘要 | A new tetracopper complex [cu(h2o)(3)cu(hcdta)](2)(clo4)(2)center dot h2o (cdta = trans-cyclohexane-1,2-diamine-n,n,n',n'-tetraacetate) has been prepared and characterized by single-crystal x-ray diffraction analysis. the crystal adopts space group c2/c with a = 16.990(10), b = 9.150(5), c = 29.318(17) angstrom, beta = 104.289(9)degrees, v = 4417(4) angstrom(3), z = 4, c28h52cl2cu4n4o31, m-r = 1265.80, d-c = 1.904 g/cm(3), mu = 2.130 mm(-1), f(000) = 2584, t = 293(2) k, the final r = 0.0328 and wr = 0.0809 for 4938 observed reflections (i > 2 sigma(i)). the tetracopper units are interconnected by weak covalent bonds into a layered structure. |
WOS关键词 | PERSPECTIVES ; MOLECULES |
WOS研究方向 | Chemistry ; Crystallography |
WOS类目 | Chemistry, Inorganic & Nuclear ; Crystallography |
语种 | 英语 |
WOS记录号 | WOS:000277342300009 |
出版者 | CHINESE JOURNAL STRUCTURAL CHEMISTRY |
URI标识 | http://www.irgrid.ac.cn/handle/1471x/2408401 |
专题 | 中国科学院大学 |
通讯作者 | Xu Li |
作者单位 | 1.Chinese Acad Sci, Fujian Inst Res Struct Matter, State Key Lab Struct Chem, Fuzhou 350002, Fujian, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China |
推荐引用方式 GB/T 7714 | Wang Mei-Xiang,Dang Zhen-Hua,Xu Li. Synthesis and crystal structure of a new tetracopper complex [cu(h2o)(3)cu(hcdta)](2)(clo4)(2)center dot h2o[J]. Chinese journal of structural chemistry,2010,29(4):551-554. |
APA | Wang Mei-Xiang,Dang Zhen-Hua,&Xu Li.(2010).Synthesis and crystal structure of a new tetracopper complex [cu(h2o)(3)cu(hcdta)](2)(clo4)(2)center dot h2o.Chinese journal of structural chemistry,29(4),551-554. |
MLA | Wang Mei-Xiang,et al."Synthesis and crystal structure of a new tetracopper complex [cu(h2o)(3)cu(hcdta)](2)(clo4)(2)center dot h2o".Chinese journal of structural chemistry 29.4(2010):551-554. |
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来源:中国科学院大学
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