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Chinese Academy of Sciences Institutional Repositories Grid
Determination of total tin and organotin compounds in shellfish by icp-ms

文献类型:期刊论文

作者Yu, Zhen-hua1,2,3; Sun, Jun-qing2; Jing, Miao2; Cao, Xuan2; Lee, Frank2; Wang, Xiao-ru2
刊名Food chemistry
出版日期2010-03-01
卷号119期号:1页码:364-367
关键词Hplc-icp-ms Organotin compounds Speciation Shellfish
ISSN号0308-8146
DOI10.1016/j.foodchem.2009.05.079
通讯作者Yu, zhen-hua(yzhhgm607@163.com)
英文摘要A method based on microwave digestion and inductively coupled plasma-mass spectrometric (icp-ms) analysis was established for the determination of total tin in shellfish samples. good linearity of the calibration curves was obtained for tin elements (r = 1.0000). detection limit for sri was 34.6 ng/g. total tin concentrations in these samples ranged from non-detectable to 0.45 mu g/g. high-performance liquid chromatography hyphenated with inductively coupled plasma-mass spectrometry (hplc-icp-ms) was applied to the simultaneous determination of five organotin compounds in the shellfish samples. the fresh and freeze-dried shellfish samples were treated by ultrasonic extraction with two different extraction solvents. four organotin compounds including dibutyltin (dbt), tributyltin (tbt), diphenyltin (dpht) and triphenyltin (tpht) in shellfish samples were detected. it was found that the dominate species in the samples were tributyltin (tbt) and triphenyltin (tpht). (c) 2009 elsevier ltd. all rights reserved
WOS关键词GAS-CHROMATOGRAPHY ; MASS SPECTROMETRY ; SPECIATION ; PRECONCENTRATION ; SEDIMENTS ; SAMPLES
WOS研究方向Chemistry ; Food Science & Technology ; Nutrition & Dietetics
WOS类目Chemistry, Applied ; Food Science & Technology ; Nutrition & Dietetics
语种英语
WOS记录号WOS:000271818200055
出版者ELSEVIER SCI LTD
URI标识http://www.irgrid.ac.cn/handle/1471x/2412649
专题中国科学院大学
通讯作者Yu, Zhen-hua
作者单位1.Chinese Acad Sci, Inst Oceanol, Qingdao, Peoples R China
2.SOA, Inst Oceanog 1, Qingdao, Peoples R China
3.Chinese Acad Sci, Grad Univ, Beijing, Peoples R China
推荐引用方式
GB/T 7714
Yu, Zhen-hua,Sun, Jun-qing,Jing, Miao,et al. Determination of total tin and organotin compounds in shellfish by icp-ms[J]. Food chemistry,2010,119(1):364-367.
APA Yu, Zhen-hua,Sun, Jun-qing,Jing, Miao,Cao, Xuan,Lee, Frank,&Wang, Xiao-ru.(2010).Determination of total tin and organotin compounds in shellfish by icp-ms.Food chemistry,119(1),364-367.
MLA Yu, Zhen-hua,et al."Determination of total tin and organotin compounds in shellfish by icp-ms".Food chemistry 119.1(2010):364-367.

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来源:中国科学院大学

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