Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry
文献类型：期刊论文
| 作者 | Cai, Yiping ; Sun, Zhiwei ; Chen, Guang ; Liu, Xiaomei ; You, Jinmao ; Zhang, Caiqing |
| 刊名 | FOOD CHEMISTRY
 |
| 出版日期 | 2016-02-01 |
| 英文摘要 | A pair of isotope-coded derivatization reagents, d(0)-10-methyl-acridone-2-sulfonyl chloride (d(0)-MASC, light form) and d(3)-10-methyl-acridone-2-sulfonyl chloride (d(3)-MASC, heavy form), were used for labeling biogenic amines (BAs). On basis of the isotope-coded derivatization, a global isotope internal standard quantitative method for determining seven BAs by high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) was developed. The d(0)-MASC and d(3)-MASC can easily label BAs under mild conditions within 15 min at 50 degrees C. The obtained light and heavy labeled BAs were monitored by the transitions of [M+H](+) -> 208 and [M+H](+) -> 211, respectively. Relative quantification of BAs was achieved by calculation of the peak area ratios of d(0)-MASC/d(3)-MASC labeled derivatives. Excellent linear responses for relative quantification were observed in the range of 1/10-10/1. The developed method has been successfully applied to the quantification of BAs in Chinese rice wine with recoveries ranging from 94.9% to 104.5%. (C) 2015 Elsevier Ltd. All rights reserved. |
| 源URL | [http://ir.nwipb.ac.cn/handle/363003/6528]  |
| 专题 | 西北高原生物研究所_中国科学院西北高原生物研究所 |
| 推荐引用方式 GB/T 7714 | Cai, Yiping,Sun, Zhiwei,Chen, Guang,et al. Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry[J]. FOOD CHEMISTRY,2016. |
| APA | Cai, Yiping,Sun, Zhiwei,Chen, Guang,Liu, Xiaomei,You, Jinmao,&Zhang, Caiqing.(2016).Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry.FOOD CHEMISTRY. |
| MLA | Cai, Yiping,et al."Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry".FOOD CHEMISTRY (2016). |
入库方式： OAI收割
来源：西北高原生物研究所
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