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Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route

文献类型：期刊论文

作者Liu, Xuebin3; Xu, Longya1; Wei, Pengfei1,2; Zhu, Xiangxue1; Wang, Yanan1,2; Chu, Weifeng1,2; Xie, Sujuan1; Yang, Zhiqiang3; Li, Xiujie1
刊名MICROPOROUS AND MESOPOROUS MATERIALS
出版日期2019-05-01
卷号279页码:220-227
ISSN号1387-1811
关键词Ferrierite Microwave Zeolite synthesis Crystallization
DOI10.1016/j.micromeso.2018.12.036
通讯作者Li, Xiujie(xiujieli@dicp.ac.cn) ; Xu, Longya(lyxu@dicp.ac.cn)
英文摘要Ferrierite (FER) zeolite has been successfully synthesized within 2-3 h through microwave assisted crystallization without using organic structure directing agent. Crystallization temperature and seed content were found to be two of the key factors. XRD patterns and SEM images of the samples taken at different periods of time revealed that seeds were only partially dissolved during the crystallization process and silicate (alumino) species in the gel grew upon the surface of the partially dissolved seed. A core-shell zeolite growth model was proposed. Compared with original seed zeolite, as-synthesized FER zeolite had more regular morphology and larger particle size. The FER crystal size could be controlled in the range of 0.4-3.0 mu m by adjusting the particle size of the seeds. FER obtained through microwave assisted rapid synthesis showed similar catalytic performance in 1-butene skeletal isomerization with the FER obtained through conventional hydrothermal synthesis.
WOS关键词SKELETAL ISOMERIZATION ; HYDROTHERMAL SYNTHESIS ; ORGANOTEMPLATE-FREE ; BETA-ZEOLITE ; FER ZEOLITE ; 1-BUTENE ; SYSTEM
资助项目National Natural Science Foundation of China[21773233] ; National Natural Science Foundation of China[21376235] ; Natural Science Foundation of Liaoning Province[201602740] ; BP Energy Innovation Laboratory
WOS研究方向Chemistry ; Science & Technology - Other Topics ; Materials Science
语种英语
出版者ELSEVIER SCIENCE BV
WOS记录号WOS:000460843500025
资助机构National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory
源URL[http://cas-ir.dicp.ac.cn/handle/321008/165888]  
专题大连化学物理研究所_中国科学院大连化学物理研究所
通讯作者Xu, Longya; Li, Xiujie
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, 457 Zhongshan Rd, Dalian 116023, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
3.BP China Dalian Off, Energy Innovat Lab, Dalian 116023, Peoples R China
推荐引用方式
GB/T 7714		 Liu, Xuebin,Xu, Longya,Wei, Pengfei,et al. Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2019,279:220-227.
APA Liu, Xuebin.,Xu, Longya.,Wei, Pengfei.,Zhu, Xiangxue.,Wang, Yanan.,...&Li, Xiujie.(2019).Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route.MICROPOROUS AND MESOPOROUS MATERIALS,279,220-227.
MLA Liu, Xuebin,et al."Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route".MICROPOROUS AND MESOPOROUS MATERIALS 279(2019):220-227.

入库方式： OAI收割

来源：大连化学物理研究所

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