Facile one-pot synthesized hydrothermal carbon from cyclodextrin: A stationary phase for hydrophilic interaction liquid chromatography
文献类型：期刊论文
| 作者 | Zhang, Hongyan1,2; Wu, Ren'an1; Zhao, Xingyun1,2; Liu, Shengju1,2; Peng, Jiaxi1,2; Li, Xin1,2; Niu, Huan1,2; Wang, Li1 |
| 刊名 | JOURNAL OF CHROMATOGRAPHY A
 |
| 出版日期 | 2019-01-25 |
| 卷号 | 1585页码:144-151 |
| ISSN号 | 0021-9673 |
| 关键词 | One-pot Hydrothermal carbon HILIC Stationary phase Polar compounds |
| DOI | 10.1016/j.chroma.2018.11.064 |
| 通讯作者 | Wu, Ren'an(wurenan@dicp.ac.cn) |
| 英文摘要 | A new hydrothermal carbon was prepared by a "one-pot" hydrothermal transformation of beta-cyclodextrin on silica microspheres (noted as silica@HTC microspheres), which was featuring as anew stationary phase for the hydrophilic interaction liquid chromatography (HILIC). The synthesized silica@HTC possessed polar groups of hydroxyl, carbonyl and carboxyl groups arising from the carbonization transformation of beta-cyclodextrin. As demonstrating great hydrophilicity, the silica@HTC was applied as an excellent HILIC stationary phase for the separation of polar compounds including phenols and the endocrine disrupting chemicals (EDCs). In comparison with commercial available HILIC stationary phases, the separation performance of the silica@HTC stationary phase was superior in the separation of phenols and EDCs. The mild hydrothermal carbon transformation of the beta-cyclodextrin on the silica microspheres in the "one-pot" manner would represent a new and simple approach to prepare a new class of saccharide-derived stationary phases by using sacharides as precursors. (C) 2018 Elsevier B.V. All rights reserved. |
| WOS关键词 | ENDOCRINE-DISRUPTING COMPOUNDS ; CARBONIZATION PROCESS ; SILICA SPHERES ; SEPARATION ; NANOPARTICLES ; NANOSPHERES ; ACIDS ; PERFORMANCE ; EXTRACTION ; PEPTIDES |
| 资助项目 | National Natural Science Foundation of China[21375125] ; National Natural Science Foundation of China[21675156] ; Instrument Developing Project of the Chinese Academy of Sciences[YZ201503] ; CAS Key Laboratory Foundation of Separation Sciences for Analytical Chemistry ; Innovation Program (DICP) of Science and Research from the Dalian Institute of Chemical Physics[TMSR201601] |
| WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
| 语种 | 英语 |
| 出版者 | ELSEVIER SCIENCE BV |
| WOS记录号 | WOS:000457507100016 |
| 资助机构 | National Natural Science Foundation of China ; National Natural Science Foundation of China ; Instrument Developing Project of the Chinese Academy of Sciences ; Instrument Developing Project of the Chinese Academy of Sciences ; CAS Key Laboratory Foundation of Separation Sciences for Analytical Chemistry ; CAS Key Laboratory Foundation of Separation Sciences for Analytical Chemistry ; Innovation Program (DICP) of Science and Research from the Dalian Institute of Chemical Physics ; Innovation Program (DICP) of Science and Research from the Dalian Institute of Chemical Physics ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Instrument Developing Project of the Chinese Academy of Sciences ; Instrument Developing Project of the Chinese Academy of Sciences ; CAS Key Laboratory Foundation of Separation Sciences for Analytical Chemistry ; CAS Key Laboratory Foundation of Separation Sciences for Analytical Chemistry ; Innovation Program (DICP) of Science and Research from the Dalian Institute of Chemical Physics ; Innovation Program (DICP) of Science and Research from the Dalian Institute of Chemical Physics ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Instrument Developing Project of the Chinese Academy of Sciences ; Instrument Developing Project of the Chinese Academy of Sciences ; CAS Key Laboratory Foundation of Separation Sciences for Analytical Chemistry ; CAS Key Laboratory Foundation of Separation Sciences for Analytical Chemistry ; Innovation Program (DICP) of Science and Research from the Dalian Institute of Chemical Physics ; Innovation Program (DICP) of Science and Research from the Dalian Institute of Chemical Physics ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Instrument Developing Project of the Chinese Academy of Sciences ; Instrument Developing Project of the Chinese Academy of Sciences ; CAS Key Laboratory Foundation of Separation Sciences for Analytical Chemistry ; CAS Key Laboratory Foundation of Separation Sciences for Analytical Chemistry ; Innovation Program (DICP) of Science and Research from the Dalian Institute of Chemical Physics ; Innovation Program (DICP) of Science and Research from the Dalian Institute of Chemical Physics |
| 源URL | [http://cas-ir.dicp.ac.cn/handle/321008/166096]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 通讯作者 | Wu, Ren'an |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, CAS Key Lab Separat Sci Analyt Chem, Dalian 116023, Peoples R China 2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhang, Hongyan,Wu, Ren'an,Zhao, Xingyun,et al. Facile one-pot synthesized hydrothermal carbon from cyclodextrin: A stationary phase for hydrophilic interaction liquid chromatography[J]. JOURNAL OF CHROMATOGRAPHY A,2019,1585:144-151. |
| APA | Zhang, Hongyan.,Wu, Ren'an.,Zhao, Xingyun.,Liu, Shengju.,Peng, Jiaxi.,...&Wang, Li.(2019).Facile one-pot synthesized hydrothermal carbon from cyclodextrin: A stationary phase for hydrophilic interaction liquid chromatography.JOURNAL OF CHROMATOGRAPHY A,1585,144-151. |
| MLA | Zhang, Hongyan,et al."Facile one-pot synthesized hydrothermal carbon from cyclodextrin: A stationary phase for hydrophilic interaction liquid chromatography".JOURNAL OF CHROMATOGRAPHY A 1585(2019):144-151. |
入库方式： OAI收割
来源：大连化学物理研究所
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