Enantiomeric separation of alpha-phenylethylamine and its derivatives by series coupled open tubular columns
文献类型：期刊论文
| 作者 | Zhou, LM; Liu, XL; Li, ZS; Wang, QH; Zhu, DQ; Hu, DH |
| 刊名 | CHINESE JOURNAL OF CHEMISTRY
 |
| 出版日期 | 1995-09-01 |
| 卷号 | 13期号:5页码:435-441 |
| 关键词 | Series Coupled Columns Modified Cyclodextrin Enantiomeric Separation Alpha-phenylethylamine And Its Derivatives |
| ISSN号 | 1001-604X |
| 文献子类 | Article |
| 英文摘要 | A series coupled fused-silica open tubular columns of a chiral and an achiral stationary phase were used to achieve the enantiomeric separation of alpha-phenylethylamine, o,m,p-methyl-and o,m,p-methoxy-alpha-phenylethylamine. A simplified equation describing the retention values of series coupled columns was derived, which relates the capacity factors of series coupled columns to the capacity factor of individual columns, their lengths, inlet and outlet pressure. Very good; agreement was obtained both between calculated values by this equation and those by Krupcik's equation and between values measured experimentally and calculated theoretically. By means of this simplified equation a computer program was developed in locating the operating range of optimum alpha(min), enantiomeric separation of all alpha-phenylethylamine and its derivatives were achieved in a single run. |
| WOS关键词 | GAS-CHROMATOGRAPHY ; CAPILLARY COLUMNS |
| WOS研究方向 | Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:A1995TU13900008 |
| 出版者 | SCIENCE CHINA PRESS |
| 源URL | [http://cas-ir.dicp.ac.cn/handle/321008/167984]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.CHINESE ACAD SCI,DALIAN INST CHEM PHYS,DALIAN 116012,LIAONING,PEOPLES R CHINA 2.FUJIAN QUANZHOU TEACHERS COLL,DEPT CHEM,QUANZHOU 362000,FUJIAN,PEOPLES R CHINA |
| 推荐引用方式 GB/T 7714 | Zhou, LM,Liu, XL,Li, ZS,et al. Enantiomeric separation of alpha-phenylethylamine and its derivatives by series coupled open tubular columns[J]. CHINESE JOURNAL OF CHEMISTRY,1995,13(5):435-441. |
| APA | Zhou, LM,Liu, XL,Li, ZS,Wang, QH,Zhu, DQ,&Hu, DH.(1995).Enantiomeric separation of alpha-phenylethylamine and its derivatives by series coupled open tubular columns.CHINESE JOURNAL OF CHEMISTRY,13(5),435-441. |
| MLA | Zhou, LM,et al."Enantiomeric separation of alpha-phenylethylamine and its derivatives by series coupled open tubular columns".CHINESE JOURNAL OF CHEMISTRY 13.5(1995):435-441. |
入库方式： OAI收割
来源：大连化学物理研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。