Enantiomeric separation of alpha-phenylethylamine and its analogs by mixed chiral and achiral stationary phase
文献类型：期刊论文
| 作者 | Zhou, LM; Liu, XL; Li, ZS; Wang, QH; Zhu, DQ; Hu, DH |
| 刊名 | CHINESE JOURNAL OF CHEMISTRY
 |
| 出版日期 | 1996 |
| 卷号 | 14期号:4页码:348-353 |
| 关键词 | Modified Cyclodextrin Enantiomeric Separation Alpha-phenylethylamine And Its Analogs |
| ISSN号 | 1001-604X |
| 文献子类 | Article |
| 英文摘要 | A mixed stationary phase of modified beta-cyclodextrin, 2,6-di-O-butyl-3-O-butyryl-beta-cyclodextrin (phase A), and SE-54 (phase B) was used for enantiomeric separation of alpha-phenylethylamine, o,m,p-methyl and o,m,p-methoxy-substituted analogs. The composition of mixed phase was selected by comparison of each calculated alpha(min)(=(gamma(m,i+1))/(gamma(m,i))), the relative retention values of the most adjacent peaks, and gamma(m,last), the relative retention values of the last eluting peak at each preselected ratio. Values of gamma(m,i), alpha calculated by derived equations were in good agreement with the experimental results obtained with two specified mixed phases. All solutes investigated a ere almost baseline separated at a predicted composition of phase A and phase B in a single run within 18 minutes. |
| WOS关键词 | GAS-CHROMATOGRAPHY |
| WOS研究方向 | Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:A1996VQ56100010 |
| 出版者 | SCIENCE CHINA PRESS |
| 源URL | [http://cas-ir.dicp.ac.cn/handle/321008/168028]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.CHINESE ACAD SCI,DALIAN INST CHEM PHYS,DALIAN 116012,LIAONING,PEOPLES R CHINA 2.FUJIAN QUANZHOU TEACHERS COLL,DEPT CHEM,QUANZHOU 362000,FUJIAN,PEOPLES R CHINA |
| 推荐引用方式 GB/T 7714 | Zhou, LM,Liu, XL,Li, ZS,et al. Enantiomeric separation of alpha-phenylethylamine and its analogs by mixed chiral and achiral stationary phase[J]. CHINESE JOURNAL OF CHEMISTRY,1996,14(4):348-353. |
| APA | Zhou, LM,Liu, XL,Li, ZS,Wang, QH,Zhu, DQ,&Hu, DH.(1996).Enantiomeric separation of alpha-phenylethylamine and its analogs by mixed chiral and achiral stationary phase.CHINESE JOURNAL OF CHEMISTRY,14(4),348-353. |
| MLA | Zhou, LM,et al."Enantiomeric separation of alpha-phenylethylamine and its analogs by mixed chiral and achiral stationary phase".CHINESE JOURNAL OF CHEMISTRY 14.4(1996):348-353. |
入库方式： OAI收割
来源：大连化学物理研究所
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