Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles
文献类型：期刊论文
| 作者 | Li, Siwei2; Yao, Siyu2; Yang, Ce1,2; Zhao, Huabo2; Lin, Lili2; Wen, Wen3; Liu, Jinxun4,5; Hu, Gang6; Li, Weixue4,5; Hou, Yanglong1 |
| 刊名 | JOURNAL OF PHYSICAL CHEMISTRY C
 |
| 出版日期 | 2017-03-09 |
| 卷号 | 121期号:9页码:5154-5160 |
| ISSN号 | 1932-7447 |
| DOI | 10.1021/acs.jpcc.7b00198 |
| 文献子类 | Article |
| 英文摘要 | Wet chemical synthesis (WCS), especially under high temperatures, is one of the most frequently used strategies for nanostructured material construction, which has been used extensively in medical-, energy-, and environment-related applications. Although knowledge about the WCS process has been accumulated in the past two decades, the high temperature used in the process and multiphase nature of intermediates and products are key factors preventing the processes from rationalization. In this paper, by using multilevel in situ cells, we developed a strategy to monitor the reaction details of WCS processed in the solid, liquid, and gas phase simultaneously. This protocol has proven successful to reconstruct the WCS process of Fe5C2 nanoparticles (NPs) and unravel the complicated chemistry in the synthesis process. |
| WOS关键词 | FISCHER-TROPSCH SYNTHESIS ; IRON CARBIDE NANOPARTICLES ; MINIMUM ENERGY PATHS ; ELASTIC BAND METHOD ; X-RAY-SCATTERING ; HYDROTHERMAL CONDITIONS ; SYNCHROTRON-RADIATION ; NANOCOMPOSITE MAGNETS ; COBALT NANOPARTICLES ; GRAPHITIC LAYERS |
| WOS研究方向 | Chemistry ; Science & Technology - Other Topics ; Materials Science |
| 语种 | 英语 |
| WOS记录号 | WOS:000396295800041 |
| 出版者 | AMER CHEMICAL SOC |
| 源URL | [http://cas-ir.dicp.ac.cn/handle/321008/169414]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 通讯作者 | Hou, Yanglong; Ma, Ding |
| 作者单位 | 1.Peking Univ, Coll Engn, Beijing 100871, Peoples R China 2.Peking Univ, Coll Chem & Mol Engn, Beijing 100871, Peoples R China 3.Chinese Acad Sci, Shanghai Inst Appl Phys, SSRF, Shanghai 201204, Peoples R China 4.Univ Sci & Technol China, Dept Chem Phys, Hefei 230026, Peoples R China 5.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China 6.Israel Chem Ltd, Shanghai 200021, Peoples R China |
| 推荐引用方式 GB/T 7714 | Li, Siwei,Yao, Siyu,Yang, Ce,et al. Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles[J]. JOURNAL OF PHYSICAL CHEMISTRY C,2017,121(9):5154-5160. |
| APA | Li, Siwei.,Yao, Siyu.,Yang, Ce.,Zhao, Huabo.,Lin, Lili.,...&Ma, Ding.(2017).Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles.JOURNAL OF PHYSICAL CHEMISTRY C,121(9),5154-5160. |
| MLA | Li, Siwei,et al."Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles".JOURNAL OF PHYSICAL CHEMISTRY C 121.9(2017):5154-5160. |
入库方式： OAI收割
来源：大连化学物理研究所
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