Efficient Separation of Four Antibacterial Diterpenes from the Roots of Salvia Prattii Using Non-Aqueous Hydrophilic Solid-Phase Extraction Followed by Preparative High-Performance Liquid Chromatography
文献类型：期刊论文
| 作者 | Dang, Jun ; Cui, Yulei ; Pei, Jinjin ; Yue, Huilan ; Liu, Zenggen ; Wang, Weidong ; Jiao, Lijin ; Mei, Lijuan ; Wang, Qilan ; Tao, Yanduo ; Shao, Yun |
| 刊名 | MOLECULES
 |
| 出版日期 | 2018-03-01 |
| 英文摘要 | An efficient preparative procedure for the separation of four antibacterial diterpenes from a Salvia prattii crude diterpenes-rich sample was developed. Firstly, the XION hydrophilic stationary phase was chosen to separate the antibacterial crude diterpenes-rich sample (18.0 g) into three fractions with a recovery of 46.1%. Then, the antibacterial fractions I (200 mg), II (200 mg), and III (150 g) were separated by the Megress C18 preparative column, and compounds tanshinone IIA (80.0 mg), salvinolone (62.0 mg), cryptotanshinone (70.0 mg), and ferruginol (68.0 mg) were produced with purities greater than 98%. The procedure achieved large-scale preparation of the four diterpenes with high purity, and it could act as a reference for the efficient preparation of active diterpenes from other plant extracts. |
| 出版者 | MDPI |
| 源URL | [http://210.75.249.4/handle/363003/13838]  |
| 专题 | 西北高原生物研究所_中国科学院西北高原生物研究所 |
| 推荐引用方式 GB/T 7714 | Dang, Jun,Cui, Yulei,Pei, Jinjin,et al. Efficient Separation of Four Antibacterial Diterpenes from the Roots of Salvia Prattii Using Non-Aqueous Hydrophilic Solid-Phase Extraction Followed by Preparative High-Performance Liquid Chromatography[J]. MOLECULES,2018. |
| APA | Dang, Jun.,Cui, Yulei.,Pei, Jinjin.,Yue, Huilan.,Liu, Zenggen.,...&Shao, Yun.(2018).Efficient Separation of Four Antibacterial Diterpenes from the Roots of Salvia Prattii Using Non-Aqueous Hydrophilic Solid-Phase Extraction Followed by Preparative High-Performance Liquid Chromatography.MOLECULES. |
| MLA | Dang, Jun,et al."Efficient Separation of Four Antibacterial Diterpenes from the Roots of Salvia Prattii Using Non-Aqueous Hydrophilic Solid-Phase Extraction Followed by Preparative High-Performance Liquid Chromatography".MOLECULES (2018). |
入库方式： OAI收割
来源：西北高原生物研究所
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