High-yield synthesis of SnO2 nanobelts by water-assisted chemical vapor deposition for sensor applications
文献类型:期刊论文
作者 | Zhang, Jing Bo1; Li, Xiao Ning1,2,3; Bai, Shou Li2; Luo, Rui Xian2; Chen, Ai Fan2; Lin, Yuan3 |
刊名 | MATERIALS RESEARCH BULLETIN
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出版日期 | 2012-11-01 |
卷号 | 47期号:11页码:3277-3282 |
关键词 | Semiconductor Nanostructures Vapor Deposition Semiconductivity |
ISSN号 | 0025-5408 |
DOI | 10.1016/j.materresbull.2012.07.023 |
英文摘要 | Well-crystallized one-dimensional (1D) SnO2 nanobelts were in situ prepared using a simple water-assisted chemical vapor deposition (CVD) method. The small Sn particles with Au-modifications were used as source materials instead of big size Sn grains to ensure the high yield of SnO2 belts. The Au layer was modified on the small Sn particles by treating Sn powders in HAuCl4 solution combined with the UV irradiation. The as-prepared SnO2 nanobelts were characterized by SEM, HRTEM, XRD, EDS and XPS. These results indicate that the growth temperature plays an important role in controlling the length-to-width ratio of nanobelts. The length-to-width ratio decreases with the growth temperature from 850 degrees C to 1000 degrees C. The nanobelts prepared at 850 degrees C shows a single-crystalline tetragonal rutile phase with a high length-to-width ratio (approximately tens of microns in length and 40-70 nm in width). However, below 850 degrees C, nanobelts cannot be formed. The as-prepared nanobelts exhibited excellent sensing properties compared with SnO2 nanoparticles and high sensing selectivity towards NO2. The high sensing selectivity to NO2 is attributed to the oxygen vacancies presenting in the as-prepared nanobelts. (C) 2012 Elsevier Ltd. All rights reserved. |
语种 | 英语 |
WOS记录号 | WOS:000311865200033 |
出版者 | PERGAMON-ELSEVIER SCIENCE LTD |
源URL | [http://ir.iccas.ac.cn/handle/121111/47809] ![]() |
专题 | 中国科学院化学研究所 |
通讯作者 | Zhang, Jing Bo |
作者单位 | 1.Tianjin Normal Univ, Key Lab Inorgan Organ Hybrid Funct Mat Chem, Tianjin Key Lab Struct & Performance Funct Mol, Coll Chem,Minist Educ, Tianjin 300387, Peoples R China 2.Beijing Univ Chem Technol, State Key Lab Chem Resource Engn, Beijing 100029, Peoples R China 3.Chinese Acad Sci, Inst Chem, Key Lab Photochem, Beijing Natl Lab Mol Sci, Beijing 100190, Peoples R China |
推荐引用方式 GB/T 7714 | Zhang, Jing Bo,Li, Xiao Ning,Bai, Shou Li,et al. High-yield synthesis of SnO2 nanobelts by water-assisted chemical vapor deposition for sensor applications[J]. MATERIALS RESEARCH BULLETIN,2012,47(11):3277-3282. |
APA | Zhang, Jing Bo,Li, Xiao Ning,Bai, Shou Li,Luo, Rui Xian,Chen, Ai Fan,&Lin, Yuan.(2012).High-yield synthesis of SnO2 nanobelts by water-assisted chemical vapor deposition for sensor applications.MATERIALS RESEARCH BULLETIN,47(11),3277-3282. |
MLA | Zhang, Jing Bo,et al."High-yield synthesis of SnO2 nanobelts by water-assisted chemical vapor deposition for sensor applications".MATERIALS RESEARCH BULLETIN 47.11(2012):3277-3282. |
入库方式: OAI收割
来源:化学研究所
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