中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Facile Fabrication of Polymeric Ionic Liquid Grafted Porous Polymer Monolith for Mixed-Mode High Performance Liquid Chromatography

文献类型:期刊论文

作者Li, Yaping1,2; Qi, Li1; Shen, Ying1,2; Zhang, Haizhi1,2; Ma, Huimin1
刊名CHINESE JOURNAL OF CHEMISTRY
出版日期2014-07-01
卷号32期号:7页码:619-625
关键词Porous Polymer Monolith Ionic Liquid Mixed-mode Chromatography
ISSN号1001-604X
DOI10.1002/cjoc.201400188
英文摘要A novel polymeric ionic liquid grafted porous polymer monolith has been facilely fabricated for mixed-mode chromatography. The column is prepared from poly (glycidyl methacrylate-co-ethylene dimethacrylate) monolith through hydrolyzation of the epoxy moieties into hydroxyl groups, followed by "grafting from" polymerization of ionic liquid of 1-vinyl-3-butylimidazolium chloride. Successful modification is characterized by scanning electron microscope, infrared spectroscopy, elemental analysis and mercury intrusion porosimetry. The HPLC performance of developed column is evaluated by separating acidic vitamin B analytes, neutral steroids and basic aromatic amines in mixed-mode chromatography on a single column, respectively. The ionic liquid affords the monolith with both enhanced separation ability and improved column efficiency.
语种英语
WOS记录号WOS:000339520300009
出版者WILEY-V C H VERLAG GMBH
源URL[http://ir.iccas.ac.cn/handle/121111/51561]  
专题中国科学院化学研究所
通讯作者Qi, Li
作者单位1.Chinese Acad Sci, Beijing Natl Lab Mol Sci, Inst Chem, Key Lab Analyt Chem Living Biosyst, Beijing 100190, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
推荐引用方式
GB/T 7714
Li, Yaping,Qi, Li,Shen, Ying,et al. Facile Fabrication of Polymeric Ionic Liquid Grafted Porous Polymer Monolith for Mixed-Mode High Performance Liquid Chromatography[J]. CHINESE JOURNAL OF CHEMISTRY,2014,32(7):619-625.
APA Li, Yaping,Qi, Li,Shen, Ying,Zhang, Haizhi,&Ma, Huimin.(2014).Facile Fabrication of Polymeric Ionic Liquid Grafted Porous Polymer Monolith for Mixed-Mode High Performance Liquid Chromatography.CHINESE JOURNAL OF CHEMISTRY,32(7),619-625.
MLA Li, Yaping,et al."Facile Fabrication of Polymeric Ionic Liquid Grafted Porous Polymer Monolith for Mixed-Mode High Performance Liquid Chromatography".CHINESE JOURNAL OF CHEMISTRY 32.7(2014):619-625.

入库方式: OAI收割

来源:化学研究所

浏览0
下载0
收藏0
其他版本

除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。