Structural analysis of PEKEKK(T/I) using WAXD, imaging plates and SAXS
文献类型:期刊论文
作者 | Zhang, QX; Song, JB; Ren, MQ; Wang, SY; Qiu, ZB; Zhang, HF; Mo, ZS |
刊名 | CHINESE JOURNAL OF POLYMER SCIENCE
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出版日期 | 2004-08-01 |
卷号 | 22期号:4页码:379-387 |
关键词 | Pekekk Waxd Imaging Plates Saxs Structural Analysis |
ISSN号 | 0256-7679 |
英文摘要 | Structures and crystal form transition of the novel aryl ether ketone polymer containing meta-phenylene linkage: PEKEKK(T/I) were investigated by wide angle X-ray diffraction (WAXD), imaging plates (IPs) and small angle X-ray scattering (SAXS). The energy of activation of the decomposition reaction and degree of crystallinity of PEKEKK(T/I) were determined by WAXD and thermo-gravimetric analysis (TGA), respectively. Results obtained from WAXD and IPs show that crystal forms I and II coexist in the PEKEKK(T/I) samples isothermally cold crystallized in the temperature range from 180degreesC to 240degreesC and only form I occurs in PEKEKK(T/I) samples isothermally cold crystallized at 270degreesC. The radius of gyration (Rg), thickness of microregions with electron-density fluctuations (E) and distribution of particle sizes were investigated by SAXS. |
语种 | 英语 |
WOS记录号 | WOS:000223585400012 |
出版者 | SPRINGER |
源URL | [http://ir.iccas.ac.cn/handle/121111/55687] ![]() |
专题 | 中国科学院化学研究所 |
通讯作者 | Mo, ZS |
作者单位 | Chinese Acad Sci, Changchun Inst Appl Chem, State Key Lab Polymer Phys & Chem, Changchun 130022, Peoples R China |
推荐引用方式 GB/T 7714 | Zhang, QX,Song, JB,Ren, MQ,et al. Structural analysis of PEKEKK(T/I) using WAXD, imaging plates and SAXS[J]. CHINESE JOURNAL OF POLYMER SCIENCE,2004,22(4):379-387. |
APA | Zhang, QX.,Song, JB.,Ren, MQ.,Wang, SY.,Qiu, ZB.,...&Mo, ZS.(2004).Structural analysis of PEKEKK(T/I) using WAXD, imaging plates and SAXS.CHINESE JOURNAL OF POLYMER SCIENCE,22(4),379-387. |
MLA | Zhang, QX,et al."Structural analysis of PEKEKK(T/I) using WAXD, imaging plates and SAXS".CHINESE JOURNAL OF POLYMER SCIENCE 22.4(2004):379-387. |
入库方式: OAI收割
来源:化学研究所
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