A study of NiZnCu-ferrite/SiO2 nanocomposites with different ferrite contents synthesized by sol-gel method
文献类型:期刊论文
作者 | Yan, SF; Geng, JX; Chen, JF; Yin, L; Zhou, YC; Liu, LJ; Zhou, E |
刊名 | JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS
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出版日期 | 2005-04-01 |
卷号 | 292页码:304-309 |
关键词 | Nanocomposites Nizncu-ferrite Sol-gel Mossbauer Spectra Magnetic Properties |
ISSN号 | 0304-8853 |
DOI | 10.1016/j.jmmm.2004.11.145 |
英文摘要 | Ni0.65Zn0.35Cu0.1Fe1.9O4/SiO2 nanocomposites with different weight percentages of NiZnCu-ferrite dispersed in silica matrix were successfully fabricated by the sol-gel method using tetraethylorthosilicate (TEOS) as a precursor of silica, and metal nitrates as precursors of NiZnCu ferrite. The thermal decomposition process of the dried gel was studied by thermogravimetric analysis (TGA) and differential thermal analysis (DTA). The obtained Ni0.65Zn0.35Cu0.1Fe1.9O4/SiO2 nanocomposites were characterized by X-ray diffraction (XRD), transmission electron microscope (TEM), scanning electron microscope (SEM), Mossbauer spectroscopy and vibrating sample magnetometry (VSM). The formation of stoichiometric NiZnCu-ferrite dispersed in silica matrix is confirmed when the weight percentage of ferrite is not more than 30%. Samples with higher ferrite content have small amount of alpha-Fe2O3. The transition from the paramagnetic to the ferromagnetic state is observed as the ferrite content increases from 20 to 90wt%. The magnetic properties of the nanocomposites are closely related to the ferrite content. The saturation magnetization increases with the ferrite content, while the coercivity reaches a maximum when the ferrite is 80wt% in the silica matrix. (c) 2004 Elsevier B.V. All rights reserved. |
语种 | 英语 |
WOS记录号 | WOS:000228838000039 |
出版者 | ELSEVIER SCIENCE BV |
源URL | [http://ir.iccas.ac.cn/handle/121111/55985] ![]() |
专题 | 中国科学院化学研究所 |
通讯作者 | Zhou, E |
作者单位 | Chinese Acad Sci, Grad Sch, Changchun Inst Appl Chem, State Key Lab Polymer Phys & Chem, Changchun 130022, Peoples R China |
推荐引用方式 GB/T 7714 | Yan, SF,Geng, JX,Chen, JF,et al. A study of NiZnCu-ferrite/SiO2 nanocomposites with different ferrite contents synthesized by sol-gel method[J]. JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS,2005,292:304-309. |
APA | Yan, SF.,Geng, JX.,Chen, JF.,Yin, L.,Zhou, YC.,...&Zhou, E.(2005).A study of NiZnCu-ferrite/SiO2 nanocomposites with different ferrite contents synthesized by sol-gel method.JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS,292,304-309. |
MLA | Yan, SF,et al."A study of NiZnCu-ferrite/SiO2 nanocomposites with different ferrite contents synthesized by sol-gel method".JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS 292(2005):304-309. |
入库方式: OAI收割
来源:化学研究所
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