Preparation and characterization of palladium colloidal nanoparticles by thermal decomposition of palladium acetate with microwave irradiation
文献类型：期刊论文
| 作者 | Chen, YX; He, BL; Liu, HF |
| 刊名 | JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
 |
| 出版日期 | 2005-03-01 |
| 卷号 | 21期号:2页码:187-190 |
| 关键词 | Thermal Decomposition Microwave Palladium Acetate Methylisobutylketone |
| ISSN号 | 1005-0302 |
| 英文摘要 | A series of solvent-stabilized palladium colloidal nanoparticles were prepared via thermal decomposition of palladium acetate methyl isobutyl ketone (MIBK) solution in the presence of alkali and alcohol with microwave irradiation. The colloidal nanoparticles were characterized with TEM, XPS and XRD. The average diameters of nanoparticles increase from 30 to 40 nm with the increase in concentration of palladium acetate. TEM and XRD observation demonstrated that the palladium colloidal nanoparticles were clusters agglomerated from hundreds of smaller palladium crystallines with size of 3 similar to 4 nm. The influence of the concentrations of alkali and alcohol to the particle size was also discussed. |
| 语种 | 英语 |
| WOS记录号 | WOS:000228230400010 |
| 出版者 | JOURNAL MATER SCI TECHNOL |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/57423]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | He, BL |
| 作者单位 | 1.Univ S Cent National, Hubei Key Lab Catalysis & Mat Sci, Wuhan 430074, Peoples R China 2.Chinese Acad Sci, Inst Chem, PCLCC, State Key Lab Polymer Phys & Chem, Beijing 100080, Peoples R China |
| 推荐引用方式 GB/T 7714 | Chen, YX,He, BL,Liu, HF. Preparation and characterization of palladium colloidal nanoparticles by thermal decomposition of palladium acetate with microwave irradiation[J]. JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY,2005,21(2):187-190. |
| APA | Chen, YX,He, BL,&Liu, HF.(2005).Preparation and characterization of palladium colloidal nanoparticles by thermal decomposition of palladium acetate with microwave irradiation.JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY,21(2),187-190. |
| MLA | Chen, YX,et al."Preparation and characterization of palladium colloidal nanoparticles by thermal decomposition of palladium acetate with microwave irradiation".JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY 21.2(2005):187-190. |
入库方式： OAI收割
来源：化学研究所
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