中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
One-pot synthesis of polyetherimides from bis(chlorophthalimide) and dichlorodiphenylsulfone in diphenylsulfone

文献类型:期刊论文

作者Shang, Zhenping; Lu, Changli; Zhao, Jianying; Yan, Jingling; Ding, Mengxian; Gao, Lianxun
刊名JOURNAL OF APPLIED POLYMER SCIENCE
出版日期2006-12-05
卷号102期号:5页码:4584-4588
关键词Polyetherimide Bis(Chlorophthalimide) Diphenylsulfone Dichlorodiphenylsulfone One-pot Synthesis
ISSN号0021-8995
DOI10.1002/app.25051
英文摘要Polyetherimides and copolymers have been synthesized in one pot from bis(chlorophthalimide), dichlorodiphenylsulfone, and bisphenolate using diphenylsulfone as the solvent. The inherent viscosities of the obtained polyimides are in the range of 0.32-0.72 dL/g, and the structures of polyimides were confirmed by IR and elemental analyses. All of the polyimides have good solubility in common organic solvents. The 5% weight-loss temperatures of the polyimides were 429-507 C in air. The glass transition temperatures (T3) of 4,4'-(9-fluorenylidene) diphenol-based polyimides are in the range of 253-268 degrees C. The Tg of bisphenol A-based polyimides is in the range of 198204 degrees C, while the T-g change inconspicuously when the ratios of diphenylsulfone increase. The wide-angle X-ray diffraction showed that all polyimides prepared are amorphous. (c) 2006 Wiley Periodicals, Inc.
语种英语
WOS记录号WOS:000241593700066
出版者JOHN WILEY & SONS INC
源URL[http://ir.iccas.ac.cn/handle/121111/58607]  
专题中国科学院化学研究所
通讯作者Gao, Lianxun
作者单位Chinese Acad Sci, Changchun Inst Appl Chem, State Key Lab Polymer Phys & Chem, Grad Sch, Changchun 130022, Peoples R China
推荐引用方式
GB/T 7714
Shang, Zhenping,Lu, Changli,Zhao, Jianying,et al. One-pot synthesis of polyetherimides from bis(chlorophthalimide) and dichlorodiphenylsulfone in diphenylsulfone[J]. JOURNAL OF APPLIED POLYMER SCIENCE,2006,102(5):4584-4588.
APA Shang, Zhenping,Lu, Changli,Zhao, Jianying,Yan, Jingling,Ding, Mengxian,&Gao, Lianxun.(2006).One-pot synthesis of polyetherimides from bis(chlorophthalimide) and dichlorodiphenylsulfone in diphenylsulfone.JOURNAL OF APPLIED POLYMER SCIENCE,102(5),4584-4588.
MLA Shang, Zhenping,et al."One-pot synthesis of polyetherimides from bis(chlorophthalimide) and dichlorodiphenylsulfone in diphenylsulfone".JOURNAL OF APPLIED POLYMER SCIENCE 102.5(2006):4584-4588.

入库方式: OAI收割

来源:化学研究所

浏览0
下载0
收藏0
其他版本

除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。