中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Preparation and characterization of crosslinked polysucrose microspheres

文献类型:期刊论文

作者Hou, Xin; Yang, Jing; Tang, Jincheng; Chen, Xiaomin; Wang, Xiukui; Yao, Kangde
刊名REACTIVE & FUNCTIONAL POLYMERS
出版日期2006-12-01
卷号66期号:12页码:1711-1717
关键词Polysucrose Microspheres Reversed Suspension Polymerization Epichlorohydrin
ISSN号1381-5148
DOI10.1016/j.reactfunctpolym.2006.06.009
英文摘要A series of novel crosslinked polysucrose (PS) microspheres were prepared by a two-stage polymerization. A soluble (linear and/or comb) polysucrose was firstly synthesized by solution polymerization of sucrose and epichlorohydrin (EP); then the crosslinked polysucrose microspheres were prepared by reversed suspension polymerization of soluble PS with EP in chlorobenzene containing Span 80. The characterization by OM and SEM indicates that these spherical beads in diameters with the range from 250 to 450 mu m have smooth surface. The hydrated and dry densities, equilibrium water contents, and hydroxyl loadings of PS microspheres were investigated. The equilibrium water content values of these microspheres changed from 79.6% to 94.1%, and the hydroxyl contents were 15.5-19.0 m mol/g dependent on the cross-linking degrees. (c) 2006 Elsevier B.V. All rights reserved.
语种英语
WOS记录号WOS:000242881100032
出版者ELSEVIER SCIENCE BV
源URL[http://ir.iccas.ac.cn/handle/121111/59081]  
专题中国科学院化学研究所
通讯作者Hou, Xin
作者单位1.Tianjin Univ, Sch Mat Sci & Engn, Tianjin 300072, Peoples R China
2.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China
推荐引用方式
GB/T 7714
Hou, Xin,Yang, Jing,Tang, Jincheng,et al. Preparation and characterization of crosslinked polysucrose microspheres[J]. REACTIVE & FUNCTIONAL POLYMERS,2006,66(12):1711-1717.
APA Hou, Xin,Yang, Jing,Tang, Jincheng,Chen, Xiaomin,Wang, Xiukui,&Yao, Kangde.(2006).Preparation and characterization of crosslinked polysucrose microspheres.REACTIVE & FUNCTIONAL POLYMERS,66(12),1711-1717.
MLA Hou, Xin,et al."Preparation and characterization of crosslinked polysucrose microspheres".REACTIVE & FUNCTIONAL POLYMERS 66.12(2006):1711-1717.

入库方式: OAI收割

来源:化学研究所

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