Preparation of silica and TiO2-SiO2 core-shell nanoparticles in water-in-oil microemulsion using compressed CO2 as reactant and antisolvent
文献类型：期刊论文
| 作者 | Zhang, JL; Liu, ZM; Han, BX; Li, ZH; Yang, GY; Li, JC; Chen, J |
| 刊名 | JOURNAL OF SUPERCRITICAL FLUIDS
 |
| 出版日期 | 2006 |
| 卷号 | 36期号:3页码:194-201 |
| 关键词 | Tio2-sio2 Core-shell Particles Water-in-oil Microemulsion Transmission Electronic Micrographs |
| ISSN号 | 0896-8446 |
| DOI | 10.1016/j.supflu.2005.06.002 |
| 英文摘要 | In this work, silica nanospheres were prepared in reverse micelles using compressed CO2 first as a reactant and then as an antisolvent. The transmission electronic micrographs (TEM) show that the silica nanoparticles in the size range of 3-15 nm were obtained, and their size increased with an increase in molar ratio of water to surfactant (w) and the decreased pressure. Furthermore, the TiO2-SiO2 core-shell particles were prepared by the reaction of compressed CO2 with sodium silicate on the surface of TiO2 nanoparticles in the reverse micelles. The morphologies, phase structure, interfacial interaction and the optical properties of the TiO2-SiO2 core-shell particles were characterized by transmission electronic micrographs (TEM), X-ray diffraction (XRD), X-ray photoelectron spectra (XPS) and UV-vis spectra, respectively. (c) 2005 Elsevier B.V. All rights reserved. |
| 语种 | 英语 |
| WOS记录号 | WOS:000233260700003 |
| 出版者 | ELSEVIER SCIENCE BV |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/59815]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Han, BX |
| 作者单位 | Chinese Acad Sci, Inst Chem, Ctr Mol Sci, Beijing 100080, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhang, JL,Liu, ZM,Han, BX,et al. Preparation of silica and TiO2-SiO2 core-shell nanoparticles in water-in-oil microemulsion using compressed CO2 as reactant and antisolvent[J]. JOURNAL OF SUPERCRITICAL FLUIDS,2006,36(3):194-201. |
| APA | Zhang, JL.,Liu, ZM.,Han, BX.,Li, ZH.,Yang, GY.,...&Chen, J.(2006).Preparation of silica and TiO2-SiO2 core-shell nanoparticles in water-in-oil microemulsion using compressed CO2 as reactant and antisolvent.JOURNAL OF SUPERCRITICAL FLUIDS,36(3),194-201. |
| MLA | Zhang, JL,et al."Preparation of silica and TiO2-SiO2 core-shell nanoparticles in water-in-oil microemulsion using compressed CO2 as reactant and antisolvent".JOURNAL OF SUPERCRITICAL FLUIDS 36.3(2006):194-201. |
入库方式： OAI收割
来源：化学研究所
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