Characterization of cyclo-depolymerization products of amorphous polyether ketone (sulfones) by reversed phase high performance liquid chromatography
文献类型：期刊论文
| 作者 | Wang Hong-Hua; Ding Jin-Ying; Chen Tian-Lu; Zhou Guang-Yuan |
| 刊名 | CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
 |
| 出版日期 | 2007-06-01 |
| 卷号 | 35期号:6页码:893-896 |
| 关键词 | Reversed Phase High Performance Liquid Chromatography Gradient Elution Cyclo-depolymerization Product Amorphous Polyether Ketone (Sulfones) |
| ISSN号 | 0253-3820 |
| 英文摘要 | A gradient elution method for the characterization of cyclo-depolymerization products of amorphous polyether ketone( sulfone) by reversed phase high performance liquid chromatography was proposed. On a SHIMADZU C, ODS column(150 mm x 4.6 mm, 5 mu m i. d.), using tetrahydrofuran(THF)/H2O as mobile phase with a flow rate of 1.0 mL/min and detection wavelength of 254 nm, all cyclic components were separated effectively and contents of cyclic oligomers were gained accurately. Results show that polyether ketone-C PEK-C), polyether sulfones-C ( PES-C), bisphenol A polysulfone (PBS) convert in good yield to a family of macrocycles through cyclo-depolymerization, the highest yield gets to 97. 57%. The comparison with MALDITOF-MS proves that HPLC is more suitable for characterization of cyclo-depolymerization product. |
| 语种 | 英语 |
| WOS记录号 | WOS:000247823600026 |
| 出版者 | SCIENCE CHINA PRESS |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/60549]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Zhou Guang-Yuan |
| 作者单位 | Chinese Acad Sci, Changchun Inst Appl Chem, State Key Lab Polymer Phys & Chem, Changchun 130022, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wang Hong-Hua,Ding Jin-Ying,Chen Tian-Lu,et al. Characterization of cyclo-depolymerization products of amorphous polyether ketone (sulfones) by reversed phase high performance liquid chromatography[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2007,35(6):893-896. |
| APA | Wang Hong-Hua,Ding Jin-Ying,Chen Tian-Lu,&Zhou Guang-Yuan.(2007).Characterization of cyclo-depolymerization products of amorphous polyether ketone (sulfones) by reversed phase high performance liquid chromatography.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,35(6),893-896. |
| MLA | Wang Hong-Hua,et al."Characterization of cyclo-depolymerization products of amorphous polyether ketone (sulfones) by reversed phase high performance liquid chromatography".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 35.6(2007):893-896. |
入库方式： OAI收割
来源：化学研究所
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