Synthesis of multimorphologic nanostructured SiO2 using organogelator sol-gel transcription
文献类型:期刊论文
作者 | Chang, Xueling; Li, Haibing; Yang, Yajiang; Xu, Huibi; Yang, Xiangliang; Ma, Yongmei |
刊名 | JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
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出版日期 | 2007-07-01 |
卷号 | 43期号:1页码:15-19 |
关键词 | Organogel Template Bis-(4-stearolyaminophenyl)Methane Solvent |
ISSN号 | 0928-0707 |
DOI | 10.1007/s10971-007-1555-5 |
英文摘要 | An organogelator based on 4,4'-diaminodiphe-nylmethane was synthesized facilely and its gelation ability was evaluated in various organic solvents. It gelated in 11 of 15 organic solvents tested herein, loading 3.0 wt%, indicating that it possesses a versatile gelation ability. TEM observations of its aggregation mode of xerogel in different solvents showed that it assembled into a rod-shaped morphology, a rolled-lamellar morphology, a spherical-like pearl necklace morphology, and a tubular morphology in dimethylformamide, dimethylsulfoxide, xylene, and 1-butanol, respectively. sol-gel polymerization of tetraethoxysilane was carried out in these gel systems. The TEM and SEM pictures of nanometer-level silica took on morphologies analogous to those of the organogels. The composition of nanostructured sintered SiO2 mainly consisted of Si and O through a scanning electron microscope SEM equipped with energy-dispersive x-ray spectroscopy. The supermolecular aggregation mode of the organogelator varied in different organic solvents. Multimorphologic nanostructured SiO2 materials were prepared through a sol-gel transcription with the simple-structure bis-(4-stearoylaminophenyl)methane as template in the different solvents. |
语种 | 英语 |
WOS记录号 | WOS:000247194300003 |
出版者 | SPRINGER |
源URL | [http://ir.iccas.ac.cn/handle/121111/62183] ![]() |
专题 | 中国科学院化学研究所 |
通讯作者 | Ma, Yongmei |
作者单位 | 1.Chinese Acad Sci, Ctr Mol Sci, Inst Chem, Lab New Mat, Beijing 100080, Peoples R China 2.Huazhong Univ Sci & Technol, Coll Life Sci & Technol, Inst Mat Med, Wuhan 430074, Peoples R China 3.Huazhong Univ Sci & Technol, Dept Chem, Wuhan 430074, Peoples R China |
推荐引用方式 GB/T 7714 | Chang, Xueling,Li, Haibing,Yang, Yajiang,et al. Synthesis of multimorphologic nanostructured SiO2 using organogelator sol-gel transcription[J]. JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY,2007,43(1):15-19. |
APA | Chang, Xueling,Li, Haibing,Yang, Yajiang,Xu, Huibi,Yang, Xiangliang,&Ma, Yongmei.(2007).Synthesis of multimorphologic nanostructured SiO2 using organogelator sol-gel transcription.JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY,43(1),15-19. |
MLA | Chang, Xueling,et al."Synthesis of multimorphologic nanostructured SiO2 using organogelator sol-gel transcription".JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY 43.1(2007):15-19. |
入库方式: OAI收割
来源:化学研究所
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