Shape-controlled synthesis of palladium nanocrystals by microwave irradiation
文献类型：期刊论文
| 作者 | Yu, Yanchun1; Zhao, Yanxi1; Huang, Tao1; Liu, Hanfan1,2 |
| 刊名 | PURE AND APPLIED CHEMISTRY
 |
| 出版日期 | 2009-12-01 |
| 卷号 | 81期号:12页码:2377-2385 |
| ISSN号 | 0033-4545 |
| 关键词 | Icosahedra Microwave Polyol Process Nanoparticles Palladium Tetraethylene Glycol |
| DOI | 10.1351/PAC-CON-08-11-22 |
| 英文摘要 | The controlled synthesis of Pd icosahedra in tetraethylene glycol (TEG) with H(2)PdCl(4) as a precursor and poly(vinylpyrrolidone) (PVP) as a stabilizer in the presence of an appropriate amount of KOH under microwave irradiation was demonstrated. TEG served as both solvent and reducing agent, and stable Pd icosahedra with uniform sizes and well-defined shapes could be prepared in a yield of over 90 % by microwave heating for 60 s. The sizes of Pd icosahedra can be well controlled by adjusting the concentration of the precursor H(2)PdCl(4). |
| 语种 | 英语 |
| 出版者 | INT UNION PURE APPLIED CHEMISTRY |
| WOS记录号 | WOS:000273206200015 |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/66035]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Huang, Tao |
| 作者单位 | 1.S Cent Univ Nationalities, Coll Chem & Mat Sci, Wuhan 430074, Peoples R China 2.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China |
| 推荐引用方式 GB/T 7714 | Yu, Yanchun,Zhao, Yanxi,Huang, Tao,et al. Shape-controlled synthesis of palladium nanocrystals by microwave irradiation[J]. PURE AND APPLIED CHEMISTRY,2009,81(12):2377-2385. |
| APA | Yu, Yanchun,Zhao, Yanxi,Huang, Tao,&Liu, Hanfan.(2009).Shape-controlled synthesis of palladium nanocrystals by microwave irradiation.PURE AND APPLIED CHEMISTRY,81(12),2377-2385. |
| MLA | Yu, Yanchun,et al."Shape-controlled synthesis of palladium nanocrystals by microwave irradiation".PURE AND APPLIED CHEMISTRY 81.12(2009):2377-2385. |
入库方式： OAI收割
来源：化学研究所
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