Preparation and properties of halogen-free flame retardant epoxy resins with phosphorus-containing siloxanes
文献类型：期刊论文
| 作者 | Ding, Jiapei; Tao, Zhiqiang; Zuo, Xiaobiao; Fan, Lin; Yang, Shiyong |
| 刊名 | POLYMER BULLETIN
 |
| 出版日期 | 2009-06-01 |
| 卷号 | 62期号:6页码:829-841 |
| 关键词 | Epoxy Flame Retardancy Mechanical Properties Phosphorus Silicon |
| ISSN号 | 0170-0839 |
| DOI | 10.1007/s00289-009-0052-0 |
| 英文摘要 | Novel epoxy resin modifiers, DOPO-TMDS and DOPO-DMDP were synthesized by addition reaction of divinylsiloxane with 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO). Halogen-free flame retardant epoxy resins were obtained through modification of o-cresol novolac epoxy resin cured by phenol novolac resin using DOPO-TMDS and DOPO-DMDP which were characterized by (1)H NMR, (13)C NMR, (31)P NMR and FT-IR measurements. Effects of the phosphorus-containing siloxanes on thermal stabilities, mechanical properties and flame retardant properties of the epoxy resins were investigated. The cured epoxy resins exhibited better mechanical properties and greatly improved flame retardant properties due to the presence of phosphorus-containing siloxanes. The cured epoxy resins with phosphorus loading of 2.0 wt% showed LOI values of 32-33 and achieved UL94V-0 ratings. |
| 语种 | 英语 |
| WOS记录号 | WOS:000266262700009 |
| 出版者 | SPRINGER |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/66259]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Tao, Zhiqiang |
| 作者单位 | Chinese Acad Sci, Inst Chem, Lab Adv Polymer Mat, Beijing 100190, Peoples R China |
| 推荐引用方式 GB/T 7714 | Ding, Jiapei,Tao, Zhiqiang,Zuo, Xiaobiao,et al. Preparation and properties of halogen-free flame retardant epoxy resins with phosphorus-containing siloxanes[J]. POLYMER BULLETIN,2009,62(6):829-841. |
| APA | Ding, Jiapei,Tao, Zhiqiang,Zuo, Xiaobiao,Fan, Lin,&Yang, Shiyong.(2009).Preparation and properties of halogen-free flame retardant epoxy resins with phosphorus-containing siloxanes.POLYMER BULLETIN,62(6),829-841. |
| MLA | Ding, Jiapei,et al."Preparation and properties of halogen-free flame retardant epoxy resins with phosphorus-containing siloxanes".POLYMER BULLETIN 62.6(2009):829-841. |
入库方式： OAI收割
来源：化学研究所
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