Synthesis and Characterization of a Fluorotitanophosphate (NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] with a Unique Lamella Framework
文献类型:期刊论文
作者 | Yang, Sihai1; Li, Guobao1; Liu, Wei2; Wang, Wei2; Yan, Zhimin3; Huang, Yining3; Liao, Fuhui1; Lin, Jianhua1 |
刊名 | INORGANIC CHEMISTRY
![]() |
出版日期 | 2009-06-15 |
卷号 | 48期号:12页码:5449-5453 |
ISSN号 | 0020-1669 |
DOI | 10.1021/ic900504m |
英文摘要 | (NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] (1) has been synthesized under hydrothermal conditions. The structure, the composition, and the thermal stability of 1 were determined by single-crystal X-ray diffraction; inductively coupled plasma-optical emission spectroscopy; IR spectroscopy; elemental analysis; thermogravimetric analysis-differential scanning calorimetry-mass spectrometry; and solid-state H-1, P-31, and F-19 NMR, and the phase purity of the bulk sample was checked by powder X-ray diffraction. Complex 1 is a fluorotitanophosphate having a unique lamella framework with both TiO5F octahedra and PO3OH tetrahedra on the surface of the layer, which leads to two different hydrogen bondings involving both P-OH and Ti-F groups. |
语种 | 英语 |
WOS记录号 | WOS:000266809200047 |
出版者 | AMER CHEMICAL SOC |
源URL | [http://ir.iccas.ac.cn/handle/121111/66831] ![]() |
专题 | 中国科学院化学研究所 |
通讯作者 | Li, Guobao |
作者单位 | 1.Peking Univ, BNLMS, State Key Lab Rare Earth Mat Chem & Applicat, Coll Chem & Mol Engn, Beijing 100871, Peoples R China 2.Lanzhou Univ, State Key Lab Appl Organ Chem, Coll Chem & Chem Engn, Lanzhou 730000, Gansu, Peoples R China 3.Univ Western Ontario, Dept Chem, London, ON N6A 5B7, Canada |
推荐引用方式 GB/T 7714 | Yang, Sihai,Li, Guobao,Liu, Wei,et al. Synthesis and Characterization of a Fluorotitanophosphate (NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] with a Unique Lamella Framework[J]. INORGANIC CHEMISTRY,2009,48(12):5449-5453. |
APA | Yang, Sihai.,Li, Guobao.,Liu, Wei.,Wang, Wei.,Yan, Zhimin.,...&Lin, Jianhua.(2009).Synthesis and Characterization of a Fluorotitanophosphate (NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] with a Unique Lamella Framework.INORGANIC CHEMISTRY,48(12),5449-5453. |
MLA | Yang, Sihai,et al."Synthesis and Characterization of a Fluorotitanophosphate (NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] with a Unique Lamella Framework".INORGANIC CHEMISTRY 48.12(2009):5449-5453. |
入库方式: OAI收割
来源:化学研究所
浏览0
下载0
收藏0
其他版本
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。