A new luminescence spectrometry for the determination of some beta-lactamic antibiotics
文献类型：期刊论文
| 作者 | Yang, JH; Ma, QL; Wu, X; Sun, LM; Cao, XH |
| 刊名 | ANALYTICAL LETTERS
 |
| 出版日期 | 1999 |
| 卷号 | 32期号:3页码:471-480 |
| 关键词 | Luminescence Spectrometry Beta-lactamic Antibiotics Cephalosporins Penicillins Redox Reaction |
| ISSN号 | 0003-2719 |
| 英文摘要 | A simple, rapid and sensitive luminescence spectrometry is described for the determination of some beta- lactamic antibiotics in pure form and in pharmaceutical formulations. The proposed method is based on the fact that the redox reaction between cerium(IV) and beta-lactamic antibiotics in an acidic medium to form Ce(LII), which can luminesce, and sodium has great enhancement for the luminescence intensity of Ce(III). The method permits the determination of 8.0x10(-6)-2.0x10(-3)mg/ml, 1.0x10(-5)-2.0x10(-3)mg/ml, 2.0x10(-5)-2.5x10(-3)mg/ml, and 2.0x10(-5)-3.0x10(-3)mg/ml for cepharadine, cefalexin, 6-aminopenicillanic acid (6-APA) and cefazolin respectively. Their detection limits (S/N=3) were 2.0x10(-6)mg/ml, 7.0x10(-6)mg/ml, 6.0x10(-6)mg/ml, and 8.0x10(-6)mg/ml, respectively. |
| 语种 | 英语 |
| WOS记录号 | WOS:000078956200004 |
| 出版者 | MARCEL DEKKER INC |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/75025]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Yang, JH |
| 作者单位 | 1.Shandong Univ, Dept Chem, Jinan 250100, Peoples R China 2.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China |
| 推荐引用方式 GB/T 7714 | Yang, JH,Ma, QL,Wu, X,et al. A new luminescence spectrometry for the determination of some beta-lactamic antibiotics[J]. ANALYTICAL LETTERS,1999,32(3):471-480. |
| APA | Yang, JH,Ma, QL,Wu, X,Sun, LM,&Cao, XH.(1999).A new luminescence spectrometry for the determination of some beta-lactamic antibiotics.ANALYTICAL LETTERS,32(3),471-480. |
| MLA | Yang, JH,et al."A new luminescence spectrometry for the determination of some beta-lactamic antibiotics".ANALYTICAL LETTERS 32.3(1999):471-480. |
入库方式： OAI收割
来源：化学研究所
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