Synthesis and characterization of a novel reactive ladderlike 4,4 '-phenylene ether-bridged polyvinylsiloxane
文献类型：期刊论文
| 作者 | Liu, CQ; Zhao, HT; Xie, P; Zhang, RB |
| 刊名 | JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY
 |
| 出版日期 | 2000-08-01 |
| 卷号 | 38期号:15页码:2702-2710 |
| 关键词 | Grignard Reaction Hydrolysis Polycondensation Characterization Ladderlike 4 4 ' -phenylene Ether-bridged Polyvinylsiloxane |
| ISSN号 | 0887-624X |
| 英文摘要 | A novel soluble, reactive ladderlike 4,4'-phenylene ether-bridged polyvinyl-siloxane (L) was synthesized successfully for the first time by a stepwise coupling polymerization (SCP) including hydrolysis and polycondensation. The monomer, 4,4'-bis(vinyldimethoxysilyl )phenylene ether (M), was synthesized by Grignard reaction. The structures of the monomer and the polymer were characterized by infrared spectrometry (IR), nuclear magnetic resonance (H-1 NMR, C-13 NMR, Si-29 NMR), mass spectrometry (MS), differential scanning calorimetry (DSC), X-ray diffration (XRD), and gel permeation chromatography (GPC). It is proposed from the characterization data that the polymer possesses an ordered ladderlike structure. (C) 2000 John Wiley & Sons, Inc. |
| 语种 | 英语 |
| WOS记录号 | WOS:000088202300010 |
| 出版者 | JOHN WILEY & SONS INC |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/75713]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Zhang, RB |
| 作者单位 | Chinese Acad Sci, PCLCC, Ctr Mol Sci, Inst Chem, Beijing 100080, Peoples R China |
| 推荐引用方式 GB/T 7714 | Liu, CQ,Zhao, HT,Xie, P,et al. Synthesis and characterization of a novel reactive ladderlike 4,4 '-phenylene ether-bridged polyvinylsiloxane[J]. JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY,2000,38(15):2702-2710. |
| APA | Liu, CQ,Zhao, HT,Xie, P,&Zhang, RB.(2000).Synthesis and characterization of a novel reactive ladderlike 4,4 '-phenylene ether-bridged polyvinylsiloxane.JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY,38(15),2702-2710. |
| MLA | Liu, CQ,et al."Synthesis and characterization of a novel reactive ladderlike 4,4 '-phenylene ether-bridged polyvinylsiloxane".JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY 38.15(2000):2702-2710. |
入库方式： OAI收割
来源：化学研究所
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