Modification and application of GDX203 chromatographic stationary phase
文献类型：期刊论文
| 作者 | Zhang, SF; Zou, J; Pan, PL; Yuan, GQ |
| 刊名 | ACTA POLYMERICA SINICA
 |
| 出版日期 | 2001-08-01 |
| 期号 | 4页码:513-516 |
| 关键词 | Gdx203 Nitration Gas Chromatographic Stationary Phase Methanol Carbonylation |
| ISSN号 | 1000-3304 |
| 英文摘要 | The porous polymer beads of styrene divinylbenzene copolymer (GDX203) were nitrated by different proportion of HNO3 (65 %) -H2SO4 (98 %) mixture at room temperature. The nitrogen content and nitro-group were confirmed with elementary analysis and IR spectrum. The modified GDX203 was used as chromatographic stationary phase for analysis of carbonylation products of methanol. The optimum gas chromatographic stationary phase was selected from modified GDX203 of different nitrogenous contents. The results showed that by using a modified column of proper nitrogen content all components in the reaction medium were separated at constant chromatographic temperature, especially CH3 COOCH3 and CH3I can be separated completely. The gas chromatographic analysis of five components was accomplished in 6 minutes. |
| 语种 | 英语 |
| WOS记录号 | WOS:000170584200020 |
| 出版者 | SCIENCE PRESS |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/77147]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Zhang, SF |
| 作者单位 | 1.Ningxia Univ, Dept Chem Sci & Chem Engn, Yinchuan 750021, Peoples R China 2.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhang, SF,Zou, J,Pan, PL,et al. Modification and application of GDX203 chromatographic stationary phase[J]. ACTA POLYMERICA SINICA,2001(4):513-516. |
| APA | Zhang, SF,Zou, J,Pan, PL,&Yuan, GQ.(2001).Modification and application of GDX203 chromatographic stationary phase.ACTA POLYMERICA SINICA(4),513-516. |
| MLA | Zhang, SF,et al."Modification and application of GDX203 chromatographic stationary phase".ACTA POLYMERICA SINICA .4(2001):513-516. |
入库方式： OAI收割
来源：化学研究所
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