Thiosalicylic acid-functionalized silver nanoparticles synthesized in one-phase system
文献类型:期刊论文
作者 | Tan, YW; Wang, Y; Jiang, L; Zhu, DB |
刊名 | JOURNAL OF COLLOID AND INTERFACE SCIENCE
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出版日期 | 2002-05-15 |
卷号 | 249期号:2页码:336-345 |
关键词 | Silver Nanoparticles Bimodal Distribution Surface Plasmon Absorption Ft-ir |
ISSN号 | 0021-9797 |
DOI | 10.1006/jcis.2001.8166 |
英文摘要 | A series of silver colloidal dispersions were prepared by two protocols, i.e., addition of the reductant-NaBH4 and the stabilizer-thiosalicylic acid (TSA) into Ag+ solution simultaneously or successively. The products were compared and characterized by TEM, electrochemical measurements, XPS, UV-vis, and FT-IR spectra. The size distributions of the Ag nanoparticles prepared by the former and latter protocols are bimodal and monodisperse, respectively. The analytic results of UV-vis spectra coincide with the TEM observation. A tentative explanation was given to the relationship between particle sizes and different synthetic protocols. The changes of the reduction potential of the reductant invoked a variance in particle diameter and size distribution. Electrochemical measurements corroborated our assumption. The composition information of TSA-derived silver nanoparticles was obtained from XPS and FT-IR spectroscopic measurements. (C) 2002 Elsevier Science (USA). |
语种 | 英语 |
WOS记录号 | WOS:000175431600011 |
出版者 | ACADEMIC PRESS INC ELSEVIER SCIENCE |
源URL | [http://ir.iccas.ac.cn/handle/121111/79313] ![]() |
专题 | 中国科学院化学研究所 |
通讯作者 | Tan, YW |
作者单位 | 1.Chinese Acad Sci, Inst Chem, Lab Organ Solids, Ctr Mol Sci, Beijing 100080, Peoples R China 2.Chinese Acad Sci, Inst Chem, State Key Lab Polymer Phys, Ctr Mol Sci, Beijing 100080, Peoples R China |
推荐引用方式 GB/T 7714 | Tan, YW,Wang, Y,Jiang, L,et al. Thiosalicylic acid-functionalized silver nanoparticles synthesized in one-phase system[J]. JOURNAL OF COLLOID AND INTERFACE SCIENCE,2002,249(2):336-345. |
APA | Tan, YW,Wang, Y,Jiang, L,&Zhu, DB.(2002).Thiosalicylic acid-functionalized silver nanoparticles synthesized in one-phase system.JOURNAL OF COLLOID AND INTERFACE SCIENCE,249(2),336-345. |
MLA | Tan, YW,et al."Thiosalicylic acid-functionalized silver nanoparticles synthesized in one-phase system".JOURNAL OF COLLOID AND INTERFACE SCIENCE 249.2(2002):336-345. |
入库方式: OAI收割
来源:化学研究所
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